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Vinyl ethers containing an epoxy group. XVI. Reaction of glycidol vinyloxyethyl ether with acetals

Journal Article · · J. Org. Chem. USSR (Engl. Transl.); (United States)
OSTI ID:5887668
In order to obtain branched acetals with epoxide groups (prospective monomers and intermediates) the authors investigated the reaction of acetaldehyde diethyl and di(1,1,3-trihydrotetrafluoropropyl) acetals with glycidol vinyloxyethyl ether. The addition of acetals to vinyl epoxy ethers was realized, and the first representative of compounds of this type, i.e., 9-glycidyloxy-6-ethoxy-4-methyl-3,7-dioxanonane, was obtained. It was also impossible to add a fluoroacetal to butyl vinyl ether (0.08-1.00 wt. % of catalyst CF/sub 3/COOH, BF/sub 3//times/ OEt/sub 2/, 20-80/degree/C, 0.5-3 h).
Research Organization:
Irkutsk Institute of Organic Chemistry (USSR)
OSTI ID:
5887668
Journal Information:
J. Org. Chem. USSR (Engl. Transl.); (United States), Journal Name: J. Org. Chem. USSR (Engl. Transl.); (United States) Vol. 24:5; ISSN JOCYA
Country of Publication:
United States
Language:
English

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