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U.S. Department of Energy
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Regenerative process for desulfurization of high temperature combustion and fuel gases. Quarterly progress report No. 11, October 1-December 31, 1978

Technical Report ·
DOI:https://doi.org/10.2172/5864215· OSTI ID:5864215

In the continuing search for more reactive calcium silicates, Portland cement, as an ingredient of concrete, has been identified to have favorable properties for sulfur absorption and regeneration. Various Portland cements have been studied for their reactivities for sulfation. Most of Portland cements showed equal or higher sorption reactivities than lime. Portland Type III had unusually high activity for a calcium-based sorbent. Furthermore, pellets could be formed from Portland Type III which had high resistance to attrition. Cyclic sulfation and regeneration using Portland Type III have been conducted in a TG system and there was no sign of weakening of the SO/sub 2/ sorption activity. The increased reactivity due to increased porosity of Portland cement pellet was noted by the addition of burnable carbon. The effects of both catalysis and porosity can be seen using fly ash as an additive. Sulfation and attrition tests for pellets of limestone fines with various binders have been tested. The results showed that both the strength and the sulfation reactivity were higher for pellets of the limestone fines with colloidal silica binder than for raw limestone. The effects of calcination temperature on the development of pore size and on the SO/sub 2/ sorption capacity have been investigated. It has been shown that the temperature maximum observed in a FBC can very possibly be due to pore size variations because of calcinations at different temperatures.

Research Organization:
Brookhaven National Lab., Upton, NY (USA)
DOE Contract Number:
EY-76-C-02-0016
OSTI ID:
5864215
Report Number(s):
BNL-50992
Country of Publication:
United States
Language:
English