Determination of vanadium in Saudi Arabian crude oil by inductively coupled plasma-mass spectrometry (ICP/MS)

Journal Article · Mon Jan 01 00:00:00 EST 1990 · Analytical Letters; (United States)

DOI:https://doi.org/10.1080/00032719008052523· OSTI ID:5793746

Al-Gadi, A A; Al-Swaidan, H M ^[1]

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1. King Saud Univ., Riyadh (Saudi Arabia)

Vanadium, among other elements which deposit on a cracking catalyst, affects the catalyst activity. The inductively coupled plasma as an ion source, when combined with a mass analyzer, resulted in a sensitive tool for elemental analysis (ICP/MS) at parts per billion levels in solution. This technique has ben applied for the determination of vanadium in five samples of Saudi Arabian crude oil. A nitric acid extraction procedure, using MIBK as a diluent for the oil and a standard addition method, were employed for the analysis. Recovery of added vanadium is 99-101%.

• OSTI ID: 5793746
• Journal Information: Analytical Letters; (United States), Vol. 23:9; ISSN 0003-2719
• Country of Publication: United States
• Language: English

Related Subjects

02 PETROLEUM
37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
PETROLEUM
CHEMICAL ANALYSIS
VANADIUM
MASS SPECTROSCOPY
CATALYSTS
EXPERIMENTAL DATA
METHYL ISOBUTYL KETONE
NITRIC ACID
QUANTITATIVE CHEMICAL ANALYSIS
SAMPLE PREPARATION
SAUDI ARABIA
SOLVENT EXTRACTION
ASIA
DATA
DEVELOPING COUNTRIES
ELEMENTS
ENERGY SOURCES
EXTRACTION
FOSSIL FUELS
FUELS
HYDROGEN COMPOUNDS
INFORMATION
INORGANIC ACIDS
KETONES
METALS
MIDDLE EAST
NUMERICAL DATA
ORGANIC COMPOUNDS
SEPARATION PROCESSES
SPECTROSCOPY
TRANSITION ELEMENTS
023000* - Petroleum- Properties & Composition
400102 - Chemical & Spectral Procedures