The Australian diffractometer at the Photon Factory

Journal Article · Wed Jan 01 04:00:00 EST 1992 · Review of Scientific Instruments; (United States)

DOI:https://doi.org/10.1063/1.1143202· OSTI ID:5645454

Barnea, Z ^[1]; Creagh, D C ^[2]; Davis, T J ^[3]; Garrett, R F ^[4]; Janky, S; Stevenson, A W; Wilkins, S W ^[3]

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1. School of Physics, University of Melbourne, Parkville, Vic 3052 (Australia)
2. Physics Department, University College, University of NSW Campbell, ACT 2600 (Australia)
3. CSIRO, Division of Materials Science and Technology, Locked Bag 33, Clayton, Vic 3168 (Australia)
4. ANSTO, Lucas Heights Laboratories, New Illawarra Road, Lucas Heights, NSW 2234 (Australia)

Outlined are design features of a versatile high-resolution two-axis diffractometer that is being constructed for operation at the Photon Factory as an Australian national facility. The instrument features optional use of multiple-imaging plates on a translating cassette to allow rapid recording of an almost complete range of data covering both the high-angle and small-angle scattering regime or alternatively the use of electronic detectors. The instrument will be capable of operation in various modes including the following: (i) high-resolution powder diffraction with single-channel counter and crystal analyzer, (ii) high-resolution, high-speed powder diffraction in the Debye--Scherrer mode with imaging plates as recording medium, either stationary or translating (for time-dependent studies), (iii) small-angle x-ray scattering with imaging plates as recording medium, (iv) protein crystallography in screenless Weissenberg mode, and (v) two- or three-axis single-crystal diffractometry. The salient features of the instrument are the use of a double-crystal sagittal focusing monochromator as primary monochromator together with the optional use of a condensing--collimating channel-cut (CCCC) monochromator or other channel-cut monochromator as secondary monochromator. The use of a CCCC monochromator enables fine tuning of beam position on sample, harmonic suppression, beam-condensation, and variation of wavelength bandpass. Further features include the use of high-precision incremental encoders on both axes, together with the capability of operating the whole diffractometer, including secondary monochromator and detectors, in vacuum of order 10{sup {minus}3} Torr in order to reduce absorption and parasitic scattering, and the use of a large camera radius (approximately 0.57 m) for the imaging plate cassette in order to increase angular resolution and signal to noise.

• OSTI ID: 5645454
• Journal Information: Review of Scientific Instruments; (United States), Journal Name: Review of Scientific Instruments; (United States) Vol. 63:1; ISSN RSINA; ISSN 0034-6748
• Country of Publication: United States
• Language: English

Related Subjects

440101* -- Radiation Instrumentation-- General Detectors or Monitors & Radiometric Instruments
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
DEBYE-SCHERRER METHOD
DESIGN
DIFFRACTION METHODS
DIFFRACTOMETERS
KEK PHOTON FACTORY
MEASURING INSTRUMENTS
MONOCHROMATORS
OPERATION
ORGANIC COMPOUNDS
PROTEINS
RADIATION SOURCES
RESOLUTION
SCATTERING
SIGNAL-TO-NOISE RATIO
SMALL ANGLE SCATTERING
SYNCHROTRON RADIATION SOURCES
X-RAY DIFFRACTOMETERS