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U.S. Department of Energy
Office of Scientific and Technical Information

Process for demetallization of heavy crudes using a catalyst having high metal retention capacity and good stability

Patent ·
OSTI ID:5622283

This patent describes a process for the hydrotreatment of heavy crudes and residues containing high levels of metals, sulphur, asphaltenes and Conradson carbon. This process consists of providing a catalyst formed by impregnating an alumina carrier in an aqueous solution containing a component selected from the metallic elements of Group VIB of the Periodic Table, a component selected from the metallic elements of Group VIII of the Periodic Table and a phosphorus oxide component and contacting the heavy crude with the catalyst in a hydrotreatment zone in the presence of hydrogen so as to convert the heavy crude into a light hydrocarbon. The phosphorus oxide is added in substantially stoichiometric quantities with respect to the metallic elements of Group VIB of the Periodic Table such that the ratio of phosphorus oxide to the oxide of the metallic elements of Group VIB on the surface of the catalyst is substantially unity. The catalyst has a surface area of between 120 to 400 m/sup 2//g and a total pore volume of between 0.5 to 1.2 cc/g wherein between 60 and 100% of the total pore volume comprises pores having a diameter of between 60 to 300 A.

Assignee:
Intevep, S.A., Caracas
Patent Number(s):
US 4579649
OSTI ID:
5622283
Country of Publication:
United States
Language:
English