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Reaction of hexafluorobutadiene with. cap alpha. -methoxystyrene

Journal Article · · Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States)
OSTI ID:5582566

Products of the (2 + 2) and (2 + 4) cyclo addition are formed in the thermal reaction of hexafluorobutadience with a-methoxystyrene. These products are primary products and do not interconvert under the reaction conditions. NMR spectroscopy showed that the introduction of a second bulky substituent at one of the carbon atoms of the substituted cyclobutane makes the energies of the two possible conformers comparable: cis- and trans-1-frifluorovinyl-2-phenyl-2-methoxy-1,4,4-trifluorocyclobutanes exist in solution as an equilibrium mixture of two conformers in 1:4 ratio for each isomer.

Research Organization:
A.N. Nesmeyanov Institute of Heteroorganic Compounds
OSTI ID:
5582566
Journal Information:
Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States), Journal Name: Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States) Vol. 33:12, PT. 1; ISSN BACCA
Country of Publication:
United States
Language:
English

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