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The dislocation-internal friction peak. gamma. in tantalum

Journal Article · · Acta Metallurgica; (USA)
 [1];  [2];  [3]
  1. ALUSUISSE, CH-3965 Chippis (CH)
  2. Ecole Polytechnique Federale, Lausanne (Switzerland)
  3. Postfach 7000, D-7250 Leonberg (DE)

Torsion-pendulum measurements were carried out on high-purity single crystal specimens of tantalum, having extremely low oxygen contents (<1 at. ppm), and on similar specimens doped with small, controlled amounts of oxygen (7 at. ppm). Our investigations are mainly concerned with the {gamma} peak, which is usually explained by kink-pair formation in screw dislocations, and with the {gamma}/sub 2/ peak, which appears close to {gamma} is small traces of oxygen are presents. The {gamma}/sub 2/ peak was formerly explained as a dislocation-enhanced Snoek peak . The {gamma} peak recovers at the peak temperature, whereas the {gamma}/sub 2/ peak is more stable. On the basis of their results, and making use of earlier investigations of Rodrian and Schultz, the authors suggest that {gamma}/sub 2/ is modified {gamma} relaxation, related to screw-dislocation segments, stabilized by oxygen-decorated kinks. The stability of the {gamma}/sub 2/ peak allows an accurate determination of the activation energy, found to be 1.00 +- 0.03 eV. This value is distinctly lower than the activation energy of the oxygen Snoek effect (1.10 eV) and is related here to the mechanism of kink-pair formation in screw dislocations, as the original {gamma} peak. The numerical value is compatible with recent values derived from flow-stress measurements. The peak {gamma}/sub 2/ shows increasing stability with increasing oxygen content. This is explained by single- and multi-decorated kinks.

OSTI ID:
5579164
Journal Information:
Acta Metallurgica; (USA), Journal Name: Acta Metallurgica; (USA) Vol. 37:4; ISSN 0001-6160; ISSN AMETA
Country of Publication:
United States
Language:
English