Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

(Evaluation of plasma sprayed crucible coatings for melt processing copper-refractory metal alloys)

Conference ·
OSTI ID:5545368
A study was made to access the suitability of several plasma arc sprayed coatings applied to graphite for application as containment crucibles for melt processing copper-refractory metal alloys. Coatings of Ta, TaC, TaB{sub 2} and ZrO{sub 2}{center dot}8w/o Y{sub 2}O{sub 3} were evaluated and compared to uncoated graphite. The ZrO{sub 2}{center dot}8w/o Y{sub 2}O{sub 3} coating was sprayed over a tungsten bond coat. Prealloyed samples of Cu-15v/o Cr and Cu-15v/o Nb were placed within the crucibles and heated inductively to 1800{degrees}C and 2100{degrees}C, respectively. Compatibility of the coating-alloy system was evaluated by optical and scanning electron microscopy, EDS, XRD and combustion chromatography.
Research Organization:
Ames Lab., IA (United States)
Sponsoring Organization:
DOE; USDOE, Washington, DC (United States)
DOE Contract Number:
W-7405-ENG-82
OSTI ID:
5545368
Report Number(s):
IS-M-698; CONF-9206135--1; ON: DE92008912
Country of Publication:
United States
Language:
English