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Framework ordering in aluminophosphate molecular sieves studied by sup 27 Al double rotation NMR

Conference ·
OSTI ID:5531483
; ; ; ;  [1]
  1. Lawrence Berkeley Lab., CA (USA) California Univ., Berkeley, CA (USA). Dept. of Chemistry

Aluminum-27 Double Rotation NMR spectroscopy (DOR) has been used to investigate framework ordering in the aluminophosphate molecular sieves VPI-5, AlPO{sub 4}-5, and AlPO{sub 4}-8. Well resolved peaks in the {sup 27}Al DOR spectra of both hydrated and dehydrated VPI-5 allow isotropic shifts to be correlated with local framework structure. more distorted aluminum environments are reflected by broader lines in {sup 27}Al DOR spectra of AlPO{sub 4}-5 and AlPO{sub 4}-8.

Research Organization:
Lawrence Berkeley Lab., CA (USA)
Sponsoring Organization:
DOE; USDOE, Washington, DC (USA)
DOE Contract Number:
AC03-76SF00098
OSTI ID:
5531483
Report Number(s):
LBL-30454; CONF-910935--1; ON: DE91012360
Country of Publication:
United States
Language:
English