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Microstructural characterization of 5-9% chromium reduced-activation steels

Technical Report ·
DOI:https://doi.org/10.2172/543209· OSTI ID:543209
 [1];  [2]
  1. Univ. of Pittsburgh, PA (United States)
  2. Oak Ridge National Lab., TN (United States)

The microstructures of a 9Cr-2W-0.25-0.1C (9Cr-2WV), a 9Cr-2W-0.25V-0.07Ta-0.1C (9Cr-2WVTa), a 7Cr-2W-0.25V-0.07Ta-0.1C (7Cr-2WVTa), and a 5Cr-2W-0.25V-0.07Ta-0.1C (5Cr-2WVTa) steel (all compositions are in weight percent) have been characterized by Analytical Electron Microscopy (AEM) and Atom Probe Field Ion Microscopy (APFIM). The matrix in all four reduced-activation steels was 100% martensite. In the two 9Cr steels, the stable precipitates were blocky M{sub 23}C{sub 6} and small spherical MC. The two lower-chromium steels contained blocky M{sub 7}C{sub 3} and small needle-shaped carbonitrides in addition to M{sub 23}C{sub 6}. AEM and APFIM analysis revealed that in the steels containing tantalum, the majority of the tantalum was in solid solution. The experimental observations were in good agreement with phases and compositions predicted by phase equilibria calculations.

Research Organization:
Oak Ridge National Lab., TN (United States)
OSTI ID:
543209
Report Number(s):
DOE/ER--0313/22; ON: DE97008797
Country of Publication:
United States
Language:
English

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