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Reaction of N/sub 2/O/sub 5/ with H/sub 2/O on carbonaceous surfaces

Journal Article · · J. Phys. Chem.; (United States)
DOI:https://doi.org/10.1021/j100410a025· OSTI ID:5346030

The heterogeneous reaction of N/sub 2/O/sub 5/ with commercially available ground charcoal in the absence of H/sub 2/O revealed a physisorption process (..gamma.. = 3 x 10/sup -3/) together with a redox reaction generating mostly NO. Slow HNO/sub 3/ formation was the result of the interaction of N/sub 2/O/sub 5/ with H/sub 2/O that was still adsorbed after prolonged pumping at 10/sup -4/ Torr. In the presence of H/sub 2/O, the same processes with ..gamma.. = 5 x 10/sup -3/ are observed. The redox reaction dominates in the early stages of the reaction, whereas the hydrolysis gains importance later at the expense of the redox reaction. The rate law for HNO/sub 3/ generation was found to be d(HNO/sub 3/)/dt = k/sub bi/(H/sub 2/O)(N/sub 25/) with k/sub bi/, the effective bimolecular rate constants, for 10 mg of carbon being (1.6 +/- 0.3) x 10/sup -13/ cm/sup 3//s.

Research Organization:
SRI International, Menlo Park, CA
DOE Contract Number:
AC03-78EV10121
OSTI ID:
5346030
Journal Information:
J. Phys. Chem.; (United States), Journal Name: J. Phys. Chem.; (United States) Vol. 90:19; ISSN JPCHA
Country of Publication:
United States
Language:
English