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Hydrogenation of carbon monoxide over silica-supported nickel-copper and ruthenium-copper catalysts

Journal Article · · J. Phys. Chem.; (United States)
DOI:https://doi.org/10.1021/j100507a010· OSTI ID:5334652

Hydrogen adsorption on supported 0.05:1 to 1:1 copper-nickel (which forms alloys in the bulk) and copper-ruthenium (which is immiscible in the bulk) decreased linearly with increasing copper content. The derived particle sizes were in the 35-65 A. range. The reaction of carbon monoxide with hydrogen at 250/sup 0/-325/sup 0/C on these catalysts proceeded with an activation energy of 30-31 kcal/mole on both catalyst systems, at all metal ratios, and at all gas compositions tested. With increasing copper content, the activity decreased, the selectivity to methane increased, and the selectivity to higher hydrocarbons decreased, which indicated that the number of active sites in the ensemble for higher hydrocarbon formation is larger than for methane formation, i.e., the effect of dilution of the active metal with copper is only a geometric one. A ''gas-induced surface enrichment'' was observed in the 0.5:1 and 1:1 copper-ruthenium catalysts, whose activity increased by more than a factor of two before reaching steady state.

Research Organization:
Univ. Technol. Eindhoven
OSTI ID:
5334652
Journal Information:
J. Phys. Chem.; (United States), Journal Name: J. Phys. Chem.; (United States) Vol. 82:18; ISSN JPCHA
Country of Publication:
United States
Language:
English