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Exploitation of solar energy storage systems. Valence isomerization between norbornadiene and quadricyclane derivatives

Journal Article · · J. Org. Chem.; (United States)
DOI:https://doi.org/10.1021/jo00339a007· OSTI ID:5313938

Use of copper(I)-nitrogen ligand catalysts such as Ph/sub 3/PCuCl.bpy, Ph/sub 3/PCuCl.phen, Ph/sub 3/PCuCl.phtha, and Ph/sub 3/PCuBr.py enables the photochemical isomerization of norbornadiene to quadricyclane to be performed at a longer wavelength than 350 nm, at which CuCl catalyst itself cannot induce such an isomerization. Among the norbornadiene derivatives bearing various chromophores, 3-(phenylcarbamoyl)norbornadiene-2-carboxylic acid undergoes a facile and quantitative isomerization into the corresponding quadricyclane derivative in sunlight. The back-isomerization of quadricyclane to 3-(phenylcarbamoyl)norbornadiene-2-carboxylic acid proceeds quantitatively by use of catalytic amounts of Rh/sub 2/(CO)/sub 4/Cl/sub 2/.

Research Organization:
Kyoto Univ., Japan
OSTI ID:
5313938
Journal Information:
J. Org. Chem.; (United States), Journal Name: J. Org. Chem.; (United States) Vol. 46:26; ISSN JOCEA
Country of Publication:
United States
Language:
English

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