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The morphological development of the Nb sub 3 Sn phase in multifilamentary superconducting wire

Thesis/Dissertation ·
OSTI ID:5169746

Multifilamentary superconducting wire is used to produce high magnetic fields. One of the materials utilized is Nb{sub 3}Sn produced by bronze-type processes. To achieve peak properties the wire-fabrication technique and the Nb{sub 3}Sn grain morphology and composition must be optimized. This work investigated the variation in critical current of an internal-tin-processed wire and a bronze-processed wire to determine the source of the superior properties in the internal-tin wire. The internal-tin process was found to have a much higher J{sub c} at low fields, {approximately} 10T, than that produced in the bronze process. It was determined that either a temperature ramp or a multi-step heat treatment with distinct temperature steps could produce a high J{sub c}. Both heat treatments incorporate the low-temperature to high-temperature schedule which gives good critical-current properties due to its influence on the Nb{sub 3}Sn microstructure, stoichiometry, and state of atomic order. Two factors, reduced filament modulation and the increased amount of small equiaxed grains, are the primary sources of the superior properties. The upper critical field of the internal tin wire is lower than that produced in the bronze process. The lower H{sub c2} can have two origins, different strain states in the two wires or Nb{sub 3}Sn composition.

Research Organization:
California Univ., Berkeley, CA (USA)
OSTI ID:
5169746
Country of Publication:
United States
Language:
English