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U.S. Department of Energy
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Applications of photoinduced electron transfer and hydrogen abstraction reactions to chemical and electrochemical conversion processes. Progress report, September 1, 1982-August 1, 1985

Technical Report ·
OSTI ID:5159116

The studies carried out have focused on photoinduced electron transfer and hydrogen atom abstraction processes. The main thrust over the past three years has been on a study of light induced electron transfer reactions and in particular on fates of the energy rich radical ions formed in electron transfer quenching of excited states. In particular we have studied these reactions under conditions - light absorbing substrates, quenchers, media - where net chemical conversion is favored over the usual back electron transfer to return to starting materials. The first part of the progress report focuses on our efforts to control reactivity by the use of specific substrates or quenchers which favor net chemical conversion. The second part describes our studies using reaction media - in this case amylose which preferentially complexes hydrophobic molecules in aqueous solution - to alter the rates of primary and secondary photophysical events associated with light induced electron transfer and other photoreactions. Our most extensive investigations of electron transfer reactions have involved the photoreduction of indigo dyes by electron donors. We have found that three representative indigo dyes, thioindigo, N,N'-diacetylindigo and oxalylindigo, all undergo photobleaching reactions with a variety of potential reductance ranging from alcohols to amines, such as triethylamine and N-benzyl-1, 4-dihydronicotinamide. 25 refs.

Research Organization:
Rochester Univ., NY (USA). Dept. of Chemistry
DOE Contract Number:
AC02-84ER13151
OSTI ID:
5159116
Report Number(s):
DOE/ER/13151-2; ON: DE86000855
Country of Publication:
United States
Language:
English