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Controlled solidification and magnetic properties of Pr-Fe-B-Cu and Nd-Fe-B alloys

Journal Article · · Journal of Applied Physics; (United States)
DOI:https://doi.org/10.1063/1.350060· OSTI ID:5126582
; ;  [1]
  1. Department of Metallurgy and Materials, University of Birmingham, Edgbaston, B15 2TT (United Kingdom)
The as-cast microstructure of the alloys Pr{sub 20.5}Fe{sub 73.8}B{sub 3.7}Cu{sub 2} and Nd{sub 16}Fe{sub 76}B{sub 8} have been modified using a vertical floating-zone (VFZ) technique. By annealing the as-cast alloys and VFZ material at 1000 {degree}C, the magnetic properties increased substantially for Pr-Fe-B-Cu alloy. VFZ growth rates up to 38 cm/h have not been sufficient to reproduce the as-cast ingot microstructure of the Pr-Fe-B-Cu alloy. Cast magnets prepared in a very small chill mold showed the best magnetic properties, with a (BH){sub max}=98 kJ/m{sup 3}. Sintered magnets prepared using the hydrogen decrepitation process from the large grained Nd-Fe-B zoned alloys exhibit inferior squareness factors to those prepared from the as-cast ingot.
OSTI ID:
5126582
Journal Information:
Journal of Applied Physics; (United States), Journal Name: Journal of Applied Physics; (United States) Vol. 70:10; ISSN 0021-8979; ISSN JAPIA
Country of Publication:
United States
Language:
English