Heteronuclear three-dimensional NMR spectroscopy. Natural abundance sup 13 C chemical shift editing of sup 1 H- sup 1 H COSY spectra
Journal Article
·
· Journal of the American Chemical Society; (USA)
- Abbott Labs., Abbott Park, IL (USA)
It has been demonstrated that heteronuclear 3D NMR spectroscopy can be effectively applied to small molecules with {sup 13}C at natural abundance. A 78mM solution of the aminoglycoside, kanamycin A was used for this experiment. The heteronuclear 3D NMR spectroscopy is shown to be a useful method for resolving spectral overlap in all frequency domains. 10 refs., 2 figs.
- OSTI ID:
- 5092804
- Journal Information:
- Journal of the American Chemical Society; (USA), Vol. 111:2; ISSN 0002-7863
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CARBON 13
ABUNDANCE
CHEMICAL SHIFT
NMR SPECTRA
CARBON ISOTOPES
EVEN-ODD NUCLEI
ISOTOPES
LIGHT NUCLEI
NUCLEI
SPECTRA
STABLE ISOTOPES
400201* - Chemical & Physicochemical Properties
400202 - Isotope Effects
Isotope Exchange
& Isotope Separation
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CARBON 13
ABUNDANCE
CHEMICAL SHIFT
NMR SPECTRA
CARBON ISOTOPES
EVEN-ODD NUCLEI
ISOTOPES
LIGHT NUCLEI
NUCLEI
SPECTRA
STABLE ISOTOPES
400201* - Chemical & Physicochemical Properties
400202 - Isotope Effects
Isotope Exchange
& Isotope Separation