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Title: The deformation behavior of ceramic crystals subjected to very low load (nano)indentations

Journal Article · · Journal of Materials Research; (United States)
 [1]; ;  [2]
  1. Materials Division, Department of Mechanical, Materials and Manufacturing Engineering, University of Newcastle upon Tyne, Newcastle upon Tyne NE1 7RU (United Kingdom)
  2. Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37381 (United States)

The ultra-low load indentation response of ceramic single crystal surfaces (Al{sub 2}O{sub 3}, SiC, Si) has been studied with a software-controlled hardness tester (Nanoindenter) operating in the load range 2--60 mN. In all cases, scanning and transmission electron microscopy have been used to characterize the deformation structures associated with these very small-scale hardness impressions. Emphasis has been placed on correlating the deformation behavior observed for particular indentations with irregularities in recorded load-displacement curves. For carefully annealed sapphire, a threshold load (for a given indenter) was observed below which the only surface response was elastic flexure and beyond which dislocation loop nucleation occurred at, or near, the theoretical shear strength to create the indentation.

DOE Contract Number:
AC05-84OR21400
OSTI ID:
5002348
Journal Information:
Journal of Materials Research; (United States), Vol. 7:2; ISSN 0884-2914
Country of Publication:
United States
Language:
English