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Viscometric determination of the onset of asphaltene flocculation: A novel method

Journal Article · · SPE Production and Facilities
DOI:https://doi.org/10.2118/28018-PA· OSTI ID:49276
;  [1]
  1. Univ. of Illinois, Chicago, IL (United States)

A new technique for the determination of the onset of asphaltene flocculation has been developed through accurate viscosity measurements of a crude oil being diluted with a precipitating agent (n-pentane, n-heptane, n-nonane). This detection method is based on experimental observations of an increase in the viscosity of a crude oil-asphaltene-precipitating agent suspension in which asphaltene particle aggregation occurs. The key point in this development is the phenomenon of asphaltene flocculation induced by the addition of a n-paraffin hydrocarbon (i.e. n-heptane, n-pentane, n-nonane) to crude oil. The onset of asphaltene flocculation is detected graphically, and its location is enhanced by comparison of the analyte curve with a reference system. The reference system was developed using polar and non-precipitating solvents (i.e. toluene, benzene, THF).

Sponsoring Organization:
USDOE
OSTI ID:
49276
Journal Information:
SPE Production and Facilities, Journal Name: SPE Production and Facilities Journal Issue: 2 Vol. 10; ISSN 1064-668X; ISSN SPRFEZ
Country of Publication:
United States
Language:
English

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