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CRYSTALLOGRAPHIC DATA. 1,3,5-TRIAMINO-2,4,6-TRINITROBENZENE

Technical Report ·
DOI:https://doi.org/10.2172/4749628· OSTI ID:4749628
Optical and x-ray crystallographic studies were made of TATB(1,3,5- triamino-2,4,6-trinitrobenzene). Crude TATB was prepared by ammonolysis of trichlorotrinitrobenzene. Large crystals of purer TATB, used for the crystallographic studies, were prepared by slow recrystallization from hot nitrobenzene. X-ray powder patterns and microscopic examination revealed no crystalline impurities. (auth)
Research Organization:
Los Alamos Scientific Lab., N. Mex.
DOE Contract Number:
W-7405-ENG-36
NSA Number:
NSA-17-006116
OSTI ID:
4749628
Report Number(s):
TID-14533; LADC-5135
Country of Publication:
United States
Language:
English

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Related Subjects

AMMONIA
BENZENE
CHEMISTRY
CHLORINATED HYDROCARBONS
CRYSTALS
DECOMPOSITION
DIFFRACTION
IMPURITIES
MICROSCOPY
POWDERS
PREPARATION
RECRYSTALLIZATION
REFLECTION
REFRACTION
X RADIATION