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Rapid, Nondestructive Determination of Beryllium Using Van de Graaff X-Rays.

Journal Article · · Analytical Chemistry
DOI:https://doi.org/10.1021/ac60192a031· OSTI ID:4734533

A method is described for the rapid nondestructive analysis for beryllium utilizing the well known Be/sup 9/( gamma ,n)2 alpha reaction. The gamma rays were produced by conversion in a tungsten target of electrons accelerated by a Van de Graaff machine. Some of the neutrons resulting from the reaction of the gamma rays with beryllium were captured in a silver disk to produce radioactive silver isotopes. The induced radioactivity was counted with a Geiger-Muller tube apparatus and was proportional to the beryllium content of the irradiated sample. The average time required for a determination was 4 minutes. With a 20-gram sample, the limit of detection in a single determination was 0.002%. (auth)

Research Organization:
Dow Chemical Co., Pittsburg, Calif.
Sponsoring Organization:
USDOE
NSA Number:
NSA-17-014160
OSTI ID:
4734533
Journal Information:
Analytical Chemistry, Journal Name: Analytical Chemistry Journal Issue: 12 Vol. 34; ISSN 0003-2700
Publisher:
American Chemical Society (ACS)
Country of Publication:
Country unknown/Code not available
Language:
English

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