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The Preparation of Radioactive D-Galactose from Radioactive D-Glucose 1

Journal Article · · Journal of Organic Chemistry
DOI:https://doi.org/10.1021/jo01039a041· OSTI ID:4712760
D-Galactose-U-C14,4-T was prepared from D-glucoseU-C14 by conversion to 2,3: 5,6-di-O-isopropylidene Ddized to di-O-isopropylidene-4-keto D- glucose-U-C14 dimethyl acetal, which was subsequentiy reduced with lithium aluminum tritide, yielding the corresponding galactose and glucose derivatives from which the free sugars were obtained after hydrolysis.
Research Organization:
Argonne National Lab., Ill.; Univ. of Illinois Coll. of Medicine, Chicago
Sponsoring Organization:
USDOE
NSA Number:
NSA-17-028972
OSTI ID:
4712760
Report Number(s):
TID-17448; UAC-6905; 0022-3263
Journal Information:
Journal of Organic Chemistry, Journal Name: Journal of Organic Chemistry Journal Issue: 4 Vol. 28; ISSN 0022-3263
Country of Publication:
Country unknown/Code not available
Language:
English