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Growth and mechanical and tribological characterization of multi-layer hard carbon films

Conference ·
OSTI ID:459945
; ;  [1]; ;  [2]; ; ;  [3]
  1. Lawrence Livermore National Lab., CA (United States)
  2. Sandia National Labs., Albuquerque, NM (United States)
  3. Los Alamos National Lab., NM (United States)

Vacuum-arc deposition is used to deposit multilayer C films by modulating the sample bias during deposition. Effect of varying the sublayer thickness in multilayer films consisting of alternating layers of ``hard`` (68.4 GPa, -100 V bias) and ``soft`` (27.5 GPa, - 200 V bias) was investigated. Films consisting of equal thickness layers of hard and soft material and an individual layer thickness varying from 10 to 35 nm were deposited. Mechanical property measurements were obtained by finite element modeling of nanoindentation load-displacement curves. The film hardness values were about 20% below the average of the component layers and relatively independent of the layer thickness. TEM revealed deterioration of the multilayer structure when the sublayer thickness was below 15 nm due to implantation damage of the hard layers caused by the energetic C{sup +} ions of the soft layers (-2000 V bias) deposited over them. Pin-on-disk wear tests show that the wear rate drops when sublayer thickness is decreased below 20 nm and remains constant with further decreases in the layer thickness.

Research Organization:
Sandia National Labs., Albuquerque, NM (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC04-94AL85000; AC03-76SF00098
OSTI ID:
459945
Report Number(s):
SAND--97-0479C; CONF-961202--90; ON: DE97004370
Country of Publication:
United States
Language:
English

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