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High selective conversion of methane to carbon monoxide and the effects of chlorine additives in the gas and solid phases on the oxidation of methane on strontium hydroxyapatites

Journal Article · · Industrial and Engineering Chemistry Research
DOI:https://doi.org/10.1021/ie960210d· OSTI ID:452282
; ; ;  [1];  [2]
  1. Univ. of Tokushima (Japan). Dept. of Chemical Science and Technology
  2. Univ. of Waterloo, Ontario (Canada)

Selectivities to carbon monoxide higher than 90% for conversions of methane greater than 10% were obtained from the partial oxidation of methane on stoichiometric strontium hydroxyapatite (SrHAp1.67) at 873 K during 6 h on stream. However, the activities decreased gradually with increasing the time-on-stream to 78 h due to the transformation of the apatite to Sr{sub 3}(PO{sub 4}){sub 2}. With small quantities of tetrachloromethane (TCM) added to the feedstream, the high selectivity to CO was retained while the conversion suffered a marked decrease with increasing the times-on-stream. In the presence of TCM the catalytic solid consists of a complex mixture of hydroxyapatite, chlorapatite, phosphate and chloride, each of which contributes dissimilarly to the catalytic process.

Sponsoring Organization:
Natural Sciences and Engineering Research Council of Canada, Ottawa, ON (Canada)
OSTI ID:
452282
Journal Information:
Industrial and Engineering Chemistry Research, Journal Name: Industrial and Engineering Chemistry Research Journal Issue: 2 Vol. 36; ISSN IECRED; ISSN 0888-5885
Country of Publication:
United States
Language:
English