THE CHEMICAL ANALYSIS OF TERNARY ALLOYS OF PLUTONIUM WITH COBALT AND CERIUM
Technical Report
·
OSTI ID:4263653
A procedure is described for the determination of plutonium, cobalt, and cerium in their ternary alloys. The plutonium is separated from and acid solution of the alloy by absorption as the nitrate complex on anion exchange resin. The cobalt and cerium are recovered in the column effluent and determined without further separation. Cobalt is determined absorptiometrically with nitroso-R-salt and cerium by titration with potassium permanganate in pyrophosphate solution to a photometric end point. The plutonium is recovered from the column by elution with hydroxylamine hydrochloride and determined absorptiometrically using the Pu (III) color. (auth)
- Research Organization:
- United Kingdom Atomic Energy Authority. Research Group. Atomic Energy Research Establishment, Harwell, Berks, England
- NSA Number:
- NSA-13-017773
- OSTI ID:
- 4263653
- Report Number(s):
- AERE-R-2878
- Country of Publication:
- United Kingdom
- Language:
- English
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Related Subjects
ABSORPTION
ACIDITY
AMINES
ANBN
ANIONS
CHEMICAL REACTIONS
CHEMICALS
CHEMISTRY
COBALT ALLOYS
COMPLEXES
HYDROCHLORIC ACID
HYDROXIDES
HYDROXYLAMINE
ION EXCHANGE MATERIALS
MANGANESE COMPOUNDS
MANGANESE OXIDES
NITRATES
NITROSO- R SALT
PERMANGANATES
PHOSPHATES
PHOTOMETRY
PLUTONIUM ALLOYS
POTASSIUM COMPOUNDS
QUALITATIVE ANALYSIS
QUANTITATIVE ANALYSIS
RECOVERY
RESINS
SEPARATION PROCESSES
SOLUTIONS
SULFONIC ACIDS
ACIDITY
AMINES
ANBN
ANIONS
CHEMICAL REACTIONS
CHEMICALS
CHEMISTRY
COBALT ALLOYS
COMPLEXES
HYDROCHLORIC ACID
HYDROXIDES
HYDROXYLAMINE
ION EXCHANGE MATERIALS
MANGANESE COMPOUNDS
MANGANESE OXIDES
NITRATES
NITROSO- R SALT
PERMANGANATES
PHOSPHATES
PHOTOMETRY
PLUTONIUM ALLOYS
POTASSIUM COMPOUNDS
QUALITATIVE ANALYSIS
QUANTITATIVE ANALYSIS
RECOVERY
RESINS
SEPARATION PROCESSES
SOLUTIONS
SULFONIC ACIDS