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Isolation and characterization of Pr@C{sup 82} and Pr{sup 2}@C{sup 80}

Journal Article · · Journal of the American Chemical Society
DOI:https://doi.org/10.1021/ja961601m· OSTI ID:426235
;  [1]
  1. Hong Kong Univ. of Science and Tehnology, Kowloon (Hong Kong)
Pr@C{sup 82} and Pr{sup 2}@C{sup 80} have been isolated with a purity of >99.0% by an efficient solvent extraction procedure, followed by HPLC separation. UV-VIS-NIR spectra of the metallofullerenes were measured in the wavelength range from 300 to 2100 nm. The X-ray photoelectron spectra of Pr@C{sup 82} and Pr{sup 2}@C{sup 80} suggest that the Pr atoms inside the carbon cages all exist in a cationic form represented by Pr{sup 3+}. 32 refs., 5 figs.
OSTI ID:
426235
Journal Information:
Journal of the American Chemical Society, Journal Name: Journal of the American Chemical Society Journal Issue: 45 Vol. 118; ISSN JACSAT; ISSN 0002-7863
Country of Publication:
United States
Language:
English

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