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PROCESS OF FORMING PLUOTONIUM SALTS FROM PLUTONIUM EXALATES

Patent ·
OSTI ID:4252990

A process is presented for converting plutonium oxalate to other plutonium compounds by a dry conversion method. According to the process, lower valence plutonium oxalate is heated in the presence of a vapor of a volatile non- oxygenated monobasic acid, such as HCl or HF. For example, in order to produce plutonium chloride, the pure plutonium oxalate is heated to about 700 deg C in a slow stream of hydrogen plus HCl. By the proper selection of an oxidizing or reducing atmosphere, the plutonium halide product can be obtained in either the plus 3 or plus 4 valence state.

Research Organization:
Originating Research Org. not identified
NSA Number:
NSA-13-015129
Assignee:
U.S. Atomic Energy Commission
Patent Number(s):
US 2875025
OSTI ID:
4252990
Country of Publication:
United States
Language:
English

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