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STRUCTURE OF THE REACTION PRODUCT OF PHENYLACETYLENE WITH IRON PENTACARBONYL

Journal Article · · Journal of the American Chemical Society (U.S.)
DOI:https://doi.org/10.1021/ja01521a013· OSTI ID:4241804

A compound first prepared by Jones, Wailes, and Whiting in 1955 has been further studied. It is concluded from analytical data that its formula is C/sub 20/H/sub 12/ O/sub 4/Fe and not C/sub 20/H/sub 10/O/sub 4/Fe. Detailed study of the infrared spectrum and the fact that it has a dipole moment of ~3 Debye units lead to the proposal of a structure in which a diphenylcyclopentadienone is bonded by pi electrons to an Fe(CO)/sub 3/ group. (auth)

Research Organization:
Massachusetts Inst. of Tech., Cambridge
Sponsoring Organization:
USDOE
NSA Number:
NSA-13-017879
OSTI ID:
4241804
Journal Information:
Journal of the American Chemical Society (U.S.), Journal Name: Journal of the American Chemical Society (U.S.) Vol. Vol: 81; ISSN JACSA
Country of Publication:
Country unknown/Code not available
Language:
English

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