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PHOTOMETRIC TITRATION OF SCANDIUM

Journal Article · · Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed.
DOI:https://doi.org/10.1021/ac60151a618· OSTI ID:4241582

A scandium solution containing copper(IV) can be titrated photometrically in acid solution with (ethylenedinitrilo)tetraacetic acid (EDTA) in the presence of up to 60 times as much rare earth (on a molar basis). The absorbance of copper(IV)-EDTA at745 m mu is used a follow the course of the titration. Large amounts of aluminum (III), calcium (II), magnesium (II), uranium(VI). and significant amounts of iron(II) and other metal ions do not interfere. Bismuth(III), hafnium (IV), zirconium(IV), fluoride, and sulfate are the most importaant interferences. The sum of scandium(III) and thorium(IV) can be determined by this method. (auth)

Research Organization:
Iowa State Coll., Ames
Sponsoring Organization:
USDOE
NSA Number:
NSA-13-015989
OSTI ID:
4241582
Journal Information:
Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed., Journal Name: Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed. Vol. Vol: 31; ISSN ANCHA
Country of Publication:
Country unknown/Code not available
Language:
English

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