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Master sintering curve: A practical approach to sintering

Journal Article · · Journal of the American Ceramic Society
;  [1]
  1. Northwestern Univ., Evanston, IL (United States)

One of the ultimate objectives for sintering studies is to be able to predict densification results under different thermal histories for a given processing method. It has been reported that the geometric parameters related to sintering often are functions only of density for a given powder and green-body process, provided that one diffusion mechanism dominates in the sintering process. Based on this report, the concept of a master sintering curve has been developed that characterizes the sintering behavior for a given powder and green-body process regardless of the heating profiles. The formulation and construction of the master sintering of alumina is used and analyzed to demonstrate this new concept. Examples of the master sintering curves obtained from other powder systems (ZnO, nickel, Al{sub 2}O{sub 3}(5 vol% TiO{sub 2}), and Al{sub 2}O{sub 3}(5 vol% ZrO{sub 2})) are presented. When this new method is used, densification behavior can be predicted under arbitrary temperature-time excursions following a minimal set of preliminary experiments, and these predictions can be used in planning sintering strategies. Moreover, deviations from the assumption of a single mechanism can be observed readily.

Sponsoring Organization:
National Science Foundation, Washington, DC (United States)
OSTI ID:
422728
Journal Information:
Journal of the American Ceramic Society, Journal Name: Journal of the American Ceramic Society Journal Issue: 12 Vol. 79; ISSN 0002-7820; ISSN JACTAW
Country of Publication:
United States
Language:
English

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