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ANALYTICAL METHODS FOR THE ABSORPTIOMETRIC DETERMINATION OF NICKEL IN ZIRCALOY 2

Technical Report ·
OSTI ID:4217207
The alloy is dissolved in dilute hydrofluoric acid. Ammoninm citrate is added to complex the zirconium, and the pH of the solution is adjustcd approximately to pH 8. The nickel dimethyl glyoxime complex is extracted into chloroform, then back extracted into dilute hydrochloric acid. The oxidized dimethyl glyoxime complex is formed and measured absorptiometrically. (auth)
Research Organization:
United Kingdom Atomic Energy Authority. Production Group. Chemical Services Dept., Springfields, Lancs, England
NSA Number:
NSA-14-005170
OSTI ID:
4217207
Report Number(s):
PGR-29(S)
Country of Publication:
Country unknown/Code not available
Language:
English

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Related Subjects

ABSORPTION
ACIDITY
ALLOYS
AMMONIUM COMPOUNDS
CHEMISTRY
CHLORINATED HYDROCARBONS
CHLOROFORM
CITRIC ACID
COMPLEXES
DIMETHYLGLYOXIME
HYDROCHLORIC ACID
HYDROFLUORIC ACID
MEASURED VALUES
NICKEL
NICKEL COMPLEXES
ORGANIC COMPOUNDS
QUANTITATIVE ANALYSIS
SOLUTIONS
SOLVENT EXTRACTION
ZIRCALOY
ZIRCONIUM