Observation of $sup 13$C--$sup 14$N dipolar couplings in single crystals of glycine

Journal Article · Wed Oct 15 04:00:00 EDT 1975 · J. Chem. Phys., v. 63, no. 8, pp. 3676-3677

OSTI ID:4184801

Griffin, R G; Pines, A; Waugh, J S

Dipolar splittings are normally not observable because the large number of nuclear couplings usually present produces extensive broadening of the NMR lines. In this note the $sup 13$C--$sup 14$N splitting in glycine is observed by using rf fields of sufficient strength to decouple the protons from the magnetically dilute nuclei. (AIP)

• Research Organization: Francis Bitter National Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139
• NSA Number: NSA-33-002606
• OSTI ID: 4184801
• Journal Information: J. Chem. Phys., v. 63, no. 8, pp. 3676-3677, Journal Name: J. Chem. Phys., v. 63, no. 8, pp. 3676-3677; ISSN JCPSA
• Country of Publication: United States
• Language: English

Related Subjects

*CARBON 13-- ISOTOPE EFFECTS
400302* --Chemistry--Organic Chemistry--Isotope Effects
COUPLING
GLYCINE
MAGNETIC DIPOLE MOMENTS
N40220* --Chemistry--Inorganic
Organic
& Physical Chemistry--Isotopic Effects
NUCLEAR MAGNETIC RESONANCE