THE POLAROGRAPHIC DETERMINATION OF NIOBIUM IN ZIRCONIUM BASE ALLOYS
Technical Report
·
OSTI ID:4165137
A polarxgraphic method was developed for the analysis of niobium in zirconium base alloys containing tin: A sample was dissolved in a mixture of sulfuric, hydrochloric and fluoboric acids and fumdd witu sulfuric acid. The resulting sulfuric acid solution was diluted to volume, and the niobium wns determined from its peak at -0.950 v vs. SCE using a cathdde may polarograph. (auth)
- Research Organization:
- Knolls Atomic Power Lab., Schenectady, N.Y.
- DOE Contract Number:
- W-31-109-ENG-52
- NSA Number:
- NSA-14-021394
- OSTI ID:
- 4165137
- Report Number(s):
- KAPL-M-DPS-3
- Country of Publication:
- United States
- Language:
- English
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