RADIATION-INDUCED FORMATION OF ORGANOTIN COMPOUNDS
Technical Report
·
OSTI ID:4131233
Particle size of tin, ambient atmosphere, chemical structure of halide, irradiation temperature, pretreatment of tin, and additives were employed as variables in a study of the nature of the reaction between organic bromides and powdered tin in a radiation field. Temperature and tin pretreatment appeared to affect the yield to the greatest extent. Among the butyl bromide isomers the reactivity followed the order tertiary > secondary > primary. Under the best conditions found in these limited studies, i.e., temperature at 90 deg C and addition of hydrobromic acid to the halide, a G-value of approximates 600 was obtained using 1-bromobutane. (auth)
- Research Organization:
- Battelle Memorial Inst., Columbus, Ohio
- DOE Contract Number:
- W-7405-ENG-92
- NSA Number:
- NSA-18-003805
- OSTI ID:
- 4131233
- Report Number(s):
- BMI-1654
- Country of Publication:
- United States
- Language:
- English
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