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STUDIES ON ANALYTICAL METHODS FOR TRACE ELEMENTS IN METALS BY USING RADIOACTIVE ISOTOPE. III. DETERMINATION OF TANTALUM BY MEANS OF ISOTOPE DILUTION METHOD

Journal Article · · Sci. Repts. Research Insts., Tohoku Univ., Ser. A
OSTI ID:4078457

The determination of tantalum by the isotope dilution method in the presence of niobium was investigated by the use of the radioisotope Ta/sup 185/. Tantalum was separated from niobium as tantalum-tannin precipitate under the optimum conditions of a pH of 1.9 to 2.5 and a tantalum/niobium ratio of up to 1/ 50. If niobium was present in amounts 100 times or more that of tantalum, reprecipitation was needed. The reciprocal of the specific activity of tanthlum pentoxide precipitate was in a linear relation to the change in the amount of tantalum added. The recommended method gave an accurate result in the determination of tantalum in steal. (auth)

Research Organization:
Research Inst. for Iron, Steel and Other Metals, Japan
NSA Number:
NSA-15-012882
OSTI ID:
4078457
Journal Information:
Sci. Repts. Research Insts., Tohoku Univ., Ser. A, Journal Name: Sci. Repts. Research Insts., Tohoku Univ., Ser. A Vol. Vol: 11
Country of Publication:
Country unknown/Code not available
Language:
English