THE ANALYSIS OF EXHAUST PRODUCTS IN THE CHLORINATION OF PLUTONIUM OXIDE WITH PHOSGENE
Technical Report
·
OSTI ID:4009342
Conventional analytical methods were adapted to the analysis of exhaust gases from the chlorination of PuO/sub 2/ with phosgene gas. Exhaust gases from chlorination of Ce and Pu oxides were found to contain CO/sub 2/, Cl/sub 2/, CO, and unreacted phosgene. The analyses were carried out using a modified Orsat apparatus with KOH for absorbing CO/sub 2/ and COCl/sub 2/, a commercial O/sub 2/ absorbent, annmoniacal Cu/sub 2/Cl/sub 2/ solution for CO, and a NaI solution in acetone for COCl/sub 2/ absorption. Two aliquots are required since COCl/sub 2/ is absorbed with CO/sub 2/. (J.R.D.)
- Research Organization:
- General Electric Co. Hanford Atomic Products Operation, Richland, Wash.
- DOE Contract Number:
- W-31-109-ENG-52
- NSA Number:
- NSA-15-025983
- OSTI ID:
- 4009342
- Report Number(s):
- HW-59749
- Country of Publication:
- United States
- Language:
- English
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