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Reductive elimination of chlorinated ethylenes by zero-valent metals

Journal Article · · Environmental Science and Technology
DOI:https://doi.org/10.1021/es9509644· OSTI ID:380784
; ;  [1];  [2];  [3]
  1. Johns Hopkins Univ., Baltimore, MD (United States)
  2. Armstrong Lab., Tyndall Air Force Base, FL (United States)
  3. Applied Research Associates, Inc., Tyndall Air Force Base, FL (United States)

To date it does not appear to have been demonstrated in the literature that halogenated ethylenes can undergo reductive {beta}-elimination to alkynes under environmental conditions. The purpose of this paper is to provide experimental evidence that such pathways may be involved in the reaction of chloroethylenes with zero-valent metals as well as to speculate on the significance of the products that may result. Calculations indicate that reductive {beta}-elimination reactions of chloroethylenes are in fact comparable energetically to hydrogenolysis at neutral pH. Experiments were therefore initiated to assess whether {beta}-elimination reactions of chlorinated ethylenes could occur in the presence of two zero-valent metals, Fe and Zn. 76 refs., 3 figs., 1 tab.

OSTI ID:
380784
Journal Information:
Environmental Science and Technology, Journal Name: Environmental Science and Technology Journal Issue: 8 Vol. 30; ISSN 0013-936X; ISSN ESTHAG
Country of Publication:
United States
Language:
English

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