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U.S. Department of Energy
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Solid phase micro extraction - A new technique coupled with gas chromatograph for chloroethene analysis from aqueous samples

Conference ·
OSTI ID:370118
;  [1]
  1. Kerr Environmental Research Lab., Ada, OK (United States)

Once the chloroethenes (tetrachloroethene and trichloroethene) contamination occurs in the subsurface environment, they tend to retain and form a Pollution plum in the aquifer because of their recalcitrance to aerobic oxidation. Currently, the most promising bioremediation method for chlorinated compounds is through anaerobic reductive biotransformation, in which each chlorine is replaced by a hydrogen. To study the biodegradation process, it is essential to monitor tetrachloroethene and its degradation daughter products frequently. An analytical method has been modified for chloroethene analysis by gas chromatography. Solid Phase Micro Extraction technique has been used to extract aqueous sample onto a fiber and then to desorb the sample directly into a gas chromatograph injection port. The total run time is less than 17 minutes.

OSTI ID:
370118
Report Number(s):
CONF-960376--
Country of Publication:
United States
Language:
English