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Formic acid oxidation in a polymer electrolyte fuel cell: A real-time mass-spectrometry study

Journal Article · · Journal of the Electrochemical Society
DOI:https://doi.org/10.1149/1.1836961· OSTI ID:367755
; ; ;  [1]
  1. Case Western Reserve Univ., Cleveland, OH (United States)

The electro-oxidation of formic acid was studied in a direct-oxidation polymer-electrolyte fuel cell at 170 C using real-time mass spectrometry. The results are compared with those obtained for methanol oxidation under the same conditions. Formic acid was electrochemically more active than methanol on both Pt-black and Pt-Ru catalysts. The polarization potential of formic acid oxidation was ca. 90 to 100 mV lower than that of methanol. The oxidation of formic acid was dependent on the water/formic acid mole ratio. The best anode performance was obtained using a water/formic acid mole ratio of {approximately}2. In addition, Pt/Ru catalyst was more active than Pt-black for formic acid oxidation. The mass spectrometric results showed that CO{sub 2} is the only reaction product of formic acid oxidation. The results are discussed in terms of possible formic acid oxidation mechanisms.

Sponsoring Organization:
USDOE
OSTI ID:
367755
Journal Information:
Journal of the Electrochemical Society, Journal Name: Journal of the Electrochemical Society Journal Issue: 7 Vol. 143; ISSN JESOAN; ISSN 0013-4651
Country of Publication:
United States
Language:
English