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Fracture in Bulk Amorphous Alloys

Conference ·
OSTI ID:3653
The fracture behavior of a Zr-based bulk amorphous alloy, Zr-10 AI-5 Ti-17.9 Cu-14.6 Ni, was examined by transmission electron microscopy (TEM) and x-ray diffraction for any evidence of crystallization preceding crack propagation. No evidence for crystallization was found in shear bands in compression specimens or at the fracture surface in tensile specimens. In- situ TEM deformation experiments were performed to more closely examine actual crack tip regions. During the in-situ deformation experiment controlled crack growth occurred to the point where the specimen was approximately 20 {micro}m thick at which point uncontrolled crack growth occurred. No evidence of any crystallization was found at the crack tips or the crack flanks. Subsequent scanning microscope examination showed that the uncontrolled crack growth region exhibited ridges and veins that appeared to have resulted from melting. Performing the deformations, both bulk and in-situ TEM, at liquid nitrogen temperatures (LN{sub 2}) resulted in an increase in the amount of controlled crack growth. The surface roughness of the bulk regions fractured at LN{sub 2} temperatures corresponded with the roughness of the crack propagation observed during the in-situ TEM experiment, suggesting that the smooth-appearing room temperature fracture sur-faces may also be a result of localized melting.
Research Organization:
Oak Ridge National Lab., TN (US)
Sponsoring Organization:
USDOE Office of Energy Research (ER) (US)
DOE Contract Number:
AC05-96OR22464
OSTI ID:
3653
Report Number(s):
ORNL/CP-101115; KC 02 01 05 0; KC 02 01 05 0
Country of Publication:
United States
Language:
English

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