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Title: Recovery of valuable chlorosilane intermediates by a novel waste conversion process. Technical report for phase IIIA (final) and phase IIIB (progress)

Abstract

From July 1994 through May 1998, direct process residue (DPR) hydrogenolysis has been studied in the laboratory, at a small Pilot Plant, and finally at a larger Pilot Plant within Dow Corning`s Carrollton, Kentucky plant. The system reacts filtered DPR with monomer at high temperature and pressure. The process demonstrates DPR conversion up to 86%. The reaction product contains high concentrations of valuable monomers such as dimethyldichlorosilane and methyldichlorosilane. A larger DPR hydrogenolysis reactor based on these results is being designed for operation in Europe at Dow Corning`s Barry, Wales site.

Authors:
Publication Date:
Research Org.:
Dow Corning Corp., Midland, MI (United States)
Sponsoring Org.:
USDOE Assistant Secretary for Energy Efficiency and Renewable Energy, Washington, DC (United States)
OSTI Identifier:
362599
Report Number(s):
DOE/AL/99566-1
ON: DE99003404; TRN: AHC29926%%254
DOE Contract Number:
FC04-94AL99566
Resource Type:
Technical Report
Resource Relation:
Other Information: PBD: Oct 1998
Country of Publication:
United States
Language:
English
Subject:
32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATION; PROGRESS REPORT; INDUSTRIAL WASTES; WASTE MANAGEMENT; MATERIALS RECOVERY; CHEMICAL INDUSTRY; BENCH-SCALE EXPERIMENTS; PILOT PLANTS; ORGANIC CHLORINE COMPOUNDS; ORGANIC SILICON COMPOUNDS; EXPERIMENTAL DATA

Citation Formats

Anderson, K.E. Recovery of valuable chlorosilane intermediates by a novel waste conversion process. Technical report for phase IIIA (final) and phase IIIB (progress). United States: N. p., 1998. Web. doi:10.2172/362599.
Anderson, K.E. Recovery of valuable chlorosilane intermediates by a novel waste conversion process. Technical report for phase IIIA (final) and phase IIIB (progress). United States. doi:10.2172/362599.
Anderson, K.E. Thu . "Recovery of valuable chlorosilane intermediates by a novel waste conversion process. Technical report for phase IIIA (final) and phase IIIB (progress)". United States. doi:10.2172/362599. https://www.osti.gov/servlets/purl/362599.
@article{osti_362599,
title = {Recovery of valuable chlorosilane intermediates by a novel waste conversion process. Technical report for phase IIIA (final) and phase IIIB (progress)},
author = {Anderson, K.E.},
abstractNote = {From July 1994 through May 1998, direct process residue (DPR) hydrogenolysis has been studied in the laboratory, at a small Pilot Plant, and finally at a larger Pilot Plant within Dow Corning`s Carrollton, Kentucky plant. The system reacts filtered DPR with monomer at high temperature and pressure. The process demonstrates DPR conversion up to 86%. The reaction product contains high concentrations of valuable monomers such as dimethyldichlorosilane and methyldichlorosilane. A larger DPR hydrogenolysis reactor based on these results is being designed for operation in Europe at Dow Corning`s Barry, Wales site.},
doi = {10.2172/362599},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Thu Oct 01 00:00:00 EDT 1998},
month = {Thu Oct 01 00:00:00 EDT 1998}
}

Technical Report:

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