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Understanding the strength of hot-pressed nanostructured powder compacts

Journal Article · · Journal of Materials Engineering and Performance
 [1];  [2]
  1. Dept. of Energy, Albany, OR (United States). Albany Research Center
  2. Lehigh Univ., Bethlehem, PA (United States)

Attrition-milled nanostructured powders were hot pressed, and macroscopic properties of density, hardness, grain size, and strength were measured. No correlation was found between processing conditions (temperature and time) used in this study and compact properties, nor was a correlation found between the tensile (or failure) stress and density, hardness, or grain size. Variations of compact properties of unmilled powder were similar to that of milled powders. Tensile data were not well fitted to a Gaussian distribution but were well fitted to a two-parameter Weibull distribution. Thus, although the milled powder compacts had an average tensile strength greater than the unmilled powder compacts, all sample compositions fit a distribution with zero as a possible minimal stress level. Weibull analysis suggests that the tensile and compression strength is controlled by the presence of fine cracks, which may limit future engineering applications. Efforts to eliminate these cracks during hot pressing were unsuccessful.

OSTI ID:
335267
Journal Information:
Journal of Materials Engineering and Performance, Journal Name: Journal of Materials Engineering and Performance Journal Issue: 1 Vol. 8; ISSN 1059-9495; ISSN JMEPEG
Country of Publication:
United States
Language:
English

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