Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Comparative analysis of new crystal and plastic scintillators for fast and thermal neutron detection

Journal Article · · Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment

This paper considers scintillation and physical properties of efficient organic scintillators tested as single crystals and as components of plastics with pulse shape discrimination (PSD). For the first time, single crystals of 9,9-dimethyl-2-phenyl-9H-fluorene (PhF) were grown for studies of the basic scintillation properties of this new compound. Comparison to classical organic crystals, like anthracene, trans-stilbene, and p-terphenyl, and to more recently introduced organic glass showed that the new crystal belongs to a group of the most efficient scintillators, with light output exceeding that of trans-stilbene and PSD comparable to that of p-terphenyl. Furthermore, additional studies were conducted to evaluate scintillation performance and physical properties, like hardness and dye leaching, of plastic scintillators prepared with PhF, organic glass, and liquid diisopropylnaphthalene (DIPN) that were considered as examples for potential replacement of PPO (2,5-diphenyloxazole) in current commercial PSD plastic scintillators. Comparison of the highest performing plastic scintillators prepared with these dyes shows that PhF formulations produced a record light output (LO) increase of 69 % relative to EJ-200. Similar improvements obtained with 6Li-loaded formulations showed that future development of PSD plastics should not be limited to use of PPO but must involve the search and exploration of new efficient dyes that may lead to discovery of much brighter organic scintillators with improved physical properties required for fast and thermal neutron detection, fast neutron spectroscopy, and antineutrino detection applications.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA), Office of Defense Nuclear Nonproliferation
Grant/Contract Number:
AC52-07NA27344
OSTI ID:
2998659
Report Number(s):
LLNL--JRNL-2004786
Journal Information:
Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment, Journal Name: Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment Vol. 1082; ISSN 0168-9002
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (31)

Highly Efficient Non-Doped Blue Organic Light-Emitting Diodes Based on Fluorene Derivatives with High Thermal Stability journal October 2005
Highly Soluble p -Terphenyl and Fluorene Derivatives as Efficient Dopants in Plastic Scintillators for Sensitive Nuclear Material Detection journal June 2017
A scintillation counter with neutron and gamma-ray discriminators journal April 1959
Development of organic scintillators journal June 1979
Characterization of a 6Li-loaded liquid organic scintillator for fast neutron spectrometry and thermal neutron detection journal July 2013
Application of solution techniques for rapid growth of organic crystals journal January 2011
The effect of material purity on the optical and scintillation properties of solution-grown trans-stilbene crystals journal April 2013
Growth mechanisms of large, faceted crystals grown from solutions journal November 2022
The role of the secondary fluorophore in ternary plastic scintillators aiming at discriminating fast neutrons from gamma-rays journal September 2019
Plastic scintillators with efficient neutron/gamma pulse shape discrimination
  • Zaitseva, Natalia; Rupert, Benjamin L.; PaweŁczak, Iwona
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 668, p. 88-93 https://doi.org/10.1016/j.nima.2011.11.071
journal March 2012
Proton light output function and neutron efficiency of a p-terphenyl detector using a 252Cf source
  • Matei, C.; Hambsch, F. -J.; Oberstedt, S.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 676 https://doi.org/10.1016/j.nima.2011.11.076
journal June 2012
Polystyrene-based scintillator with pulse-shape discrimination capability
  • Zhmurin, P. N.; Lebedev, V. N.; Titskaya, V. D.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 761 https://doi.org/10.1016/j.nima.2014.05.084
journal October 2014
Scintillation properties of solution-grown trans-stilbene single crystals
  • Zaitseva, Natalia; Glenn, Andrew; Carman, Leslie
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 789 https://doi.org/10.1016/j.nima.2015.03.090
journal July 2015
Recent developments in plastic scintillators with pulse shape discrimination
  • Zaitseva, N. P.; Glenn, A. M.; Mabe, A. N.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 889 https://doi.org/10.1016/j.nima.2018.01.093
journal May 2018
Neutron- γ discrimination with organic scintillators: Intrinsic pulse shape and light yield contributions
  • Sénoville, M.; Delaunay, F.; Pârlog, M.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 971 https://doi.org/10.1016/j.nima.2020.164080
journal August 2020
Multiple dye interactions in plastic scintillators: Effects on pulse shape discrimination
  • Zaitseva, N. P.; Glenn, A. M.; Carman, M. L.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 978 https://doi.org/10.1016/j.nima.2020.164455
journal October 2020
Organic glass scintillator (OGS) property comparisons to Stilbene, EJ-276 and BC-404
  • Warburton, William K.; Carlson, Joseph S.; Feng, Patrick L.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1018 https://doi.org/10.1016/j.nima.2021.165778
journal December 2021
Synthesis and processing of lithium-loaded plastic scintillators on the kilogram scale
  • Ford, Michael J.; Aigeldinger, Elisabeth; Sutanto, Felicia
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1050 https://doi.org/10.1016/j.nima.2023.168093
journal May 2023
3D printable polyvinyltoluene-based plastic scintillators with pulse shape discrimination
  • Kim, Yongwook; Zaitseva, Natalia; Ford, Michael J.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1055 https://doi.org/10.1016/j.nima.2023.168537
journal October 2023
Impact of temperature on light yield and pulse shape discrimination of polysiloxane-based organic scintillators formulated with commercial resins
  • Arrue, Jonathan; Chandler, Caleb; Duce, Mackenzie
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1056 https://doi.org/10.1016/j.nima.2023.168650
journal November 2023
Performance stability of plastics for neutron-gamma pulse shape discrimination
  • Zaitseva, Natalia; Carman, Leslie; Glenn, Andrew
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1068 https://doi.org/10.1016/j.nima.2024.169731
journal November 2024
Performance of large-scale 6Li-doped pulse-shape discriminating plastic scintillators
  • Roca, C.; Bowden, N. S.; Carman, L.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 1069 https://doi.org/10.1016/j.nima.2024.169916
journal December 2024
Polysiloxane Scintillators for Efficient Neutron and Gamma-Ray Pulse Shape Discrimination journal June 2020
Plastic Scintillators via Rapid Photoinitiated Cationic Polymerization of Vinyltoluene journal May 2022
Fluorene Derivatives for Efficient Prompt Scintillation in Plastic Scintillators journal May 2022
Taking Advantage of Disorder: Small-Molecule Organic Glasses for Radiation Detection and Particle Discrimination journal July 2017
Study of Organic Scintillators journal April 1956
Distribution Coefficient of 1,4-diphenyl-1,3-butadiene in p-terphenyl Single Crystal and Its Influence on Scintillation Crystal Light Output journal July 2015
Pulse Shape Discrimination in Impure and Mixed Single-Crystal Organic Scintillators journal December 2011
Efficient Prompt Scintillation and Fast Neutron-Gamma Ray Discrimination Using Amorphous Blends of Difluorenylsilane Organic Glass and In Situ Polymerized Vinyltoluene journal September 2021
Development of a Portable Pixelated Fast-Neutron Imaging Panel journal June 2022

Similar Records

Polysiloxane Scintillators for Efficient Neutron and Gamma-Ray Pulse Shape Discrimination
Journal Article · Thu Jun 25 00:00:00 EDT 2020 · ACS Applied Polymer Materials · OSTI ID:1644046

Impact of temperature on light yield and pulse shape discrimination of polysiloxane-based organic scintillators formulated with commercial resins
Journal Article · Fri Sep 01 00:00:00 EDT 2023 · Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment · OSTI ID:2203880

3D printable polyvinyltoluene-based plastic scintillators with pulse shape discrimination
Journal Article · Sun Jul 16 00:00:00 EDT 2023 · Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment · OSTI ID:2005127