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Convergence of micro-geochemistry and micro-geomechanics towards understanding proppant shale rock interaction: A Caney shale case study in southern Oklahoma, USA

Journal Article · · Journal of Natural Gas Science and Engineering
 [1];  [2];  [3];  [4];  [3];  [1];  [5];  [1]
  1. Oklahoma State University, Stillwater, OK (United States)
  2. Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
  3. University of Pittsburgh, PA (United States)
  4. Oklahoma Geological Survey, Norman, OK (United States)
  5. Continental Resources, Inc., Oklahoma City, OK (United States)

As a direct outcome of economic development coupled with an increase in population, global energy demand will continue to rise in the coming decades. Although renewable energy sources are increasingly investigated for optimal production, the immediate needs require focus on energy sources that are currently available and reliable, with a minimal environmental impact; the efficient exploration and production of unconventional hydrocarbon resources is bridging the energy needs and energy aspirations, during the current energy transition period. The main challenges are related to the accurate quantification of the critical rock properties that influence production, their heterogeneity and the multiscale driven physico-chemical nature of rock–fluid interactions. A key feature of shale reservoirs is their low permeability due to dominating nanoporosity of the clay-rich matrix. As a means of producing these reservoirs in a cost-effective manner, a prerequisite is creation of hydraulic fracture networks capable of the highest level of continued conductivity. Fracturing fluid chemical design, formation brine geochemical composition, and rock mineralogy all contribute to swelling-induced conductivity damage. The Caney Shale is an organic-rich, often calcareous mudrock. Many studies have examined the impact that clay has on different kinds of shale productivity but there is currently no data reported on the Caney Shale in relation to horizontal drilling; all reported data on the Caney Shale is on vertical wells which are shallow, compared to an emerging play that is at double the depth. Here, in this work we develop geochemical–geomechanical integration of rock properties at micro-and nanoscales that can provide insights into the potential proppant embedment and its mitigation. The novel methodology amalgamates the following: computed X-ray tomography, scanning electron microscopy, energy dispersive spectroscopy, micro-indentation, and Raman spectroscopy techniques. Here, our results show that due to the multiscale heterogeneity in the Caney Shale, these geochemical and structural properties translate into a variation in mechanical properties that will impact interaction between the proppant and the host shale rock.

Research Organization:
National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)
Sponsoring Organization:
USDOE Office of Fossil Energy and Carbon Management (FECM)
Grant/Contract Number:
FE0031776; AC02-05CH11231
OSTI ID:
2997269
Alternate ID(s):
OSTI ID: 1833093
OSTI ID: 1906817
Journal Information:
Journal of Natural Gas Science and Engineering, Journal Name: Journal of Natural Gas Science and Engineering Vol. 96; ISSN 1875-5100
Publisher:
Elsevier BVCopyright Statement
Country of Publication:
United States
Language:
English

References (44)

An Experimental Investigation of Shale Mechanical Properties Through Drained and Undrained Test Mechanisms journal March 2013
Mechanical Behavior of Shale at Different Strain Rates journal April 2019
Experimental deformation of shale: Mechanical properties and microstructural indicators of mechanisms journal December 1993
The trend in current and near future energy consumption from a statistical perspective journal December 2000
A review of the technical and economic evaluation techniques for shale gas development journal June 2015
Optimal thermal and thermodynamic performance of a solar parabolic trough receiver with different nanofluids and at different concentration ratios journal May 2017
The shale gas revolution: Barriers, sustainability, and emerging opportunities journal August 2017
Multi-scale multi-dimensional microstructure imaging of oil shale pyrolysis using X-ray micro-tomography, automated ultra-high resolution SEM, MAPS Mineralogy and FIB-SEM journal September 2017
Land-based wind energy cost trends in Germany, Denmark, Ireland, Norway, Sweden and the United States journal November 2020
An overview of TOUGH-based geomechanics models journal November 2017
Assessing low-maturity organic matter in shales using Raman spectroscopy: Effects of sample preparation and operating procedure journal April 2018
Interplay between pore connectivity and permeability in shale sample journal March 2020
Rock characterization of Fayetteville shale gas plays journal March 2013
Projection of world fossil fuels by country journal February 2015
Nanoscale pore structure characterization of the Bakken shale in the USA journal December 2017
Nanoscale rock mechanical property changes in heterogeneous coal after water adsorption journal April 2018
A review of liquid nitrogen fracturing technology journal April 2020
Coupling dynamic in situ X-ray micro-imaging and indentation: A novel approach to evaluate micromechanics applied to oil shale journal September 2021
Effective application of proppants during the hydraulic fracturing of coal seam gas reservoirs: Implications from laboratory testings of propped and unpropped coal fractures journal November 2021
Benchmark study of undrained triaxial testing of Opalinus Clay shale: Results and implications for robust testing journal March 2021
Carbon dioxide storage potential of shales journal July 2008
CT scanning and flow measurements of shale fractures after multiple shearing events journal December 2017
Mineralogical characterization and macro/microstrain analysis of the Marcellus shales journal October 2020
Observations of breakage for transversely isotropic shale using acoustic emission and X-ray computed tomography: Effect of bedding orientation, pre-existing weaknesses, and pore water journal March 2021
Indentation size effects in the nano- and micro-hardness of fcc single crystal metals journal October 2006
Low temperature in-situ micro-compression testing of iron pillars journal December 2016
Laboratory characterisation of shale properties journal June 2012
Advanced laboratory techniques characterising solids, fluids and pores in shales journal September 2019
Insight into the nanoscale pore structure of organic-rich shales in the Bakken Formation, USA journal August 2020
An optimized model of calculating optimal packing ratio for graded proppant placement with consideration of proppant embedment and deformation journal January 2021
Characterization of two types of shale rocks from Guizhou China through micro-indentation, statistical and machine-learning tools journal January 2022
Quantitative mineralogy for facies definition in the Marcellus Shale (Appalachian Basin, USA) using XRD-XRF integration journal September 2018
Raman analysis of DLC and Si-DLC films deposited on nitrile rubber journal October 2013
Raman Spectroscopy Analysis of the Structure and Surface Chemistry of Ti 3 C 2 T x MXene journal April 2020
Multimodal Visualization of Vaca Muerta Shale Fabric Before and After Maturation journal May 2021
Integration of Multiscale Imaging of Nanoscale Pore Microstructures in Gas Shales journal June 2021
Direct Detection of Oil Shale Yields: A Laser-Induced Voltage Investigation journal January 2019
The transition from planar to en echelon morphology in a single vein in shale: Insights from X-ray computed tomography scanning journal February 2020
Evaluation of variable gas saturation on acoustic log data from the Haynesville Shale gas play, NW Louisiana, USA journal March 2011
Spectrum of pore types and networks in mudrocks and a descriptive classification for matrix-related mudrock pores journal June 2012
Wettability of Mississippian Barnett Shale samples at different depths: Investigations from directional spontaneous imbibition journal January 2016
An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments journal June 1992
Improving People’s Lives: The Case for Hydraulic Fracturing journal February 2016
Microscale Chemistry: Raman Analysis of Fluid and Melt Inclusions journal April 2020