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Crystal and molecular structure of the ethylenediamine complex [Tc(CO){sub 3}Br{center_dot}en]

Journal Article · · Radiochemistry
OSTI ID:28600
An X-ray structure analysis is completed for the ethylenediamine complex [Tc(CO){sub 3}Br{center_dot}en]. The crystals belong to the monoclinic system, a = 7.013(1), b = 13.177(8), c = 10.736(5) {angstrom}, {beta} = 101.73(3){degrees}, space group P2{sub 1}/n, Z = 4, d{sub calc} = 2.19 g/cm{sup 3}. The crystal lattice is constructed of isolated [Tc(CO){sub 3}Br{center_dot}en] molecules with the facial configuration. The total energy and bond multiplicities are calculated by the extended Hueckel method for this complex, its chloride analog, and their hypothetical meridional isomers.
OSTI ID:
28600
Journal Information:
Radiochemistry, Journal Name: Radiochemistry Journal Issue: 3 Vol. 36; ISSN RDIOEO; ISSN 1066-3622
Country of Publication:
United States
Language:
English