Synthesis of 3,3-dinitroazetidine
Patent
·
OSTI ID:27696
The compound, 3,3-dinitroazetidine, and a process of preparing 3,3-dinitroazetidine are described including reacting a mixture of 1-tertiary-butyl-3,3-dinitroazetidine and benzyl chloroformate to form 1-(benzyloxycarbonyl)-3,3-dinitroazetidine, reacting the 1-(benzyloxycarbonyl)-3,3-dinitroazetidine and trifluoromethanesulfonic acid to form 3,3-dinitroazetidinium trifluoromethanesulfonate, and neutralizing the 3,3-dinitroazetidinium trifluoromethanesulfonate with a base to form 3,3-dinitroazetidine. Salts of the 3,3-dinitroazetidine and preparation of such salts are also disclosed. 1 fig.
- Assignee:
- Dept. of Energy, Washington, DC (United States)
- Patent Number(s):
- US 5,395,945/A/
- Application Number:
- PAN: 8-037,873
- OSTI ID:
- 27696
- Country of Publication:
- United States
- Language:
- English
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