High resolution characterization of soil dissolved organic matter with FTICR-MS (Fourier-transform ion cyclotron resonance mass spectrometry) from soil samples in control and warming plots in Blodgett Forest, CA (2014 and 2018)

Dataset · Tue Dec 31 23:00:00 EST 2024

DOI:https://doi.org/10.15485/2569200· OSTI ID:2569200

Karaoz, Ulas ^[1]; J. Eloy Alves, Ricardo ^[1]; Chu, Rosalie ^[2]; K. Eder, Elizabeth ^[2]; Nicora, Carrie ^[2]; Torn, Margaret ^[1]; L. Brodie, Eoin ^[1]

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1. Lawrence Berkeley National Laboratory
2. Pacific Northwest National Laboratory (PNNL)

The pathways of carbon transport and loss through and from soils—soil organic matter (SOM) depolymerization to dissolved organic carbon and mineralization to carbon dioxide (CO2)—are fundamentally driven by microbial activity, which is strongly regulated by environmental conditions. As part of Lawrence Berkeley National Laboratory (LBNL) Terrestrial Ecosystem Science (TES) Belowground Biogeochemistry Science Focus Area (SFA), we have established a novel whole-soil long-term warming experiment at the University of California (UC) Blodgett Forest Research Station (Sierra Nevada) in 2014, where we study the role of biogeochemical, microbial and geochemical process interactions in SOM decomposition and stabilization.This package contains Fourier transform ion cyclotron resonance mass spectrometry (21 Tesla FTICR-MS) data measured in negative and positive ionization mode from water and methanol soil extracts. Soil samples were collected in 2014/06/03 and 2018/06/04 from 3 replicated paired plots that had been subjected to experimental warming since June 2014 to simulate a predicted climate change scenario for northern California. The following files are included: (1) fticr_neg_h2oMeoh_data_raw.csv: raw data from combined water (H2O) and methanol (MeOH) extracts in negative ion mode, (2) fticr_neg_h2oMeoh_data_processed.csv: processed data from combined water (H2O) and methanol (MeOH) extracts in negative ion mode, (3) fticr_neg_metadata.csv: metadata for samples/measurements in negative ion mode, (4) fticr_pos_h2oMeoh_data_raw.csv: raw data from combined water (H2O) and methanol (MeOH) extracts in positive ion mode, (5) fticr_pos_h2oMeoh_data_processed.csv: processed data from combined water (H2O) and methanol (MeOH) extracts in positive ion mode, (6) fticr_pos_metadata.csv: metadata for samples/measurements in positive ion mode.

• Research Organization: Belowground Biogeochemistry Scientific Focus Area
• Sponsoring Organization: U.S. DOE > Office of Science > Biological and Environmental Research (BER)
• DOE Contract Number: AC02-05CH11231
• OSTI ID: 2569200
• Country of Publication: United States
• Language: English

Related Subjects

54 ENVIRONMENTAL SCIENCES
Belowground Biogeochemistry Science Focus Area
Blodgett Forest Research Station
EARTH SCIENCE > LAND SURFACE > SOILS
FTICR-MS
Fourier transform ion cyclotron resonance mass spectrometry
METABOLOMICS
Terrestrial Ecosystem Science (TES)
dissolved organic matter
metabolomics
methanol
soil metabolomics
soil organic matter
soil warming