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Ultrasonic characterization of slurries in an autoclave reactor at elevated temperature

Journal Article · · Industrial and Engineering Chemistry Research
DOI:https://doi.org/10.1021/ie950771p· OSTI ID:256852
; ; ; ; ;  [1]
  1. USDOE Pittsburgh Energy Technology Center, PA (United States)

The application of the three-phase slurry reactor system for coal liquefaction processing and chemical industries has recently received considerable attention. To design and efficiently operate a three-phase slurry reactor, the degree of dispersion of the solid (catalyst) in the reactor must be understood and controlled. An ultrasonic technique was developed to measure the concentration of solids in an autoclave reactor. Preliminary measurements were conducted on slurries consisting of molten paraffin wax, glass beads, and nitrogen bubbles at 189 C. The data show that the velocity and attenuation of the sound are well-defined functions of the solid and gas concentrations in the molten wax. The results suggest possibilities for directly measuring solids concentration during operation of a three-phase slurry reactor.

OSTI ID:
256852
Journal Information:
Industrial and Engineering Chemistry Research, Journal Name: Industrial and Engineering Chemistry Research Journal Issue: 6 Vol. 35; ISSN IECRED; ISSN 0888-5885
Country of Publication:
United States
Language:
English

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