Recent advances in characterization of rechargeable battery materials via scanning probe microscopy

Russell, Joshua A.; Davis, Paul H.; Efaw, Corey M.; Xiong, Hui

doi:10.1039/D4TA05975A

Recent advances in characterization of rechargeable battery materials via scanning probe microscopy

Journal Article · Tue Feb 18 00:00:00 EST 2025 · Journal of Materials Chemistry. A

DOI:https://doi.org/10.1039/D4TA05975A· OSTI ID:2500997

^[1]; ^[1]; Efaw, Corey M. ^[1]; ^[1]

Micron School of Materials Science and Engineering, Boise State University, Boise, ID, 83725, USA

Scanning probe microscopy can be used to obtain topographical, mechanical, electrical, and electrochemical information on a wide range of materials in a variety of environments, including in situ and operando studies for rechargeable battery systems.

View Accepted Manuscript (Publisher)

Sponsoring Organization:: USDOE

Grant/Contract Number:: SC0019121

OSTI ID:: 2500997

Journal Information:: Journal of Materials Chemistry. A, Journal Name: Journal of Materials Chemistry. A Journal Issue: 8 Vol. 13; ISSN JMCAET; ISSN 2050-7488

Publisher:: Royal Society of Chemistry (RSC)Copyright Statement

Country of Publication:: United Kingdom

Language:: English

References (135)

High-Voltage Lithium-Metal Batteries Enabled by Localized High-Concentration Electrolytes Chen, Shuru; Zheng, Jianming; Mei, Donghai Advanced Materials, Vol. 30, Issue 21 https://doi.org/10.1002/adma.201706102	journal	March 2018
Sodium and Sodium-Ion Batteries: 50 Years of Research Delmas, Claude Advanced Energy Materials, Vol. 8, Issue 17 https://doi.org/10.1002/aenm.201703137	journal	February 2018
Recent Progress in Understanding Solid Electrolyte Interphase on Lithium Metal Anodes Wu, Haiping; Jia, Hao; Wang, Chongmin Advanced Energy Materials, Vol. 11, Issue 5 https://doi.org/10.1002/aenm.202003092	journal	December 2020
Characterizing Batteries by In Situ Electrochemical Atomic Force Microscopy: A Critical Review Zhang, Zhenyu; Said, Samia; Smith, Keenan Advanced Energy Materials, Vol. 11, Issue 38 https://doi.org/10.1002/aenm.202101518	journal	September 2021
Spatiotemporal Changes of the Solid Electrolyte Interphase in Lithium-Ion Batteries Detected by Scanning Electrochemical Microscopy Bülter, Heinz; Peters, Fabian; Schwenzel, Julian Angewandte Chemie International Edition, Vol. 53, Issue 39 https://doi.org/10.1002/anie.201403935	journal	July 2014
From Lithium-Ion to Sodium-Ion Batteries: Advantages, Challenges, and Surprises Nayak, Prasant Kumar; Yang, Liangtao; Brehm, Wolfgang Angewandte Chemie International Edition, Vol. 57, Issue 1 https://doi.org/10.1002/anie.201703772	journal	November 2017
A Flexible Solid Electrolyte Interphase Layer for Long-Life Lithium Metal Anodes Li, Nian-Wu; Shi, Yang; Yin, Ya-Xia Angewandte Chemie International Edition, Vol. 57, Issue 6 https://doi.org/10.1002/anie.201710806	journal	January 2018
Correlative Electrochemical Microscopy of Li‐Ion (De)intercalation at a Series of Individual LiMn ₂ O ₄ Particles Tao, Binglin; Yule, Lewis C.; Daviddi, Enrico Angewandte Chemie International Edition, Vol. 58, Issue 14 https://doi.org/10.1002/anie.201814505	journal	February 2019
Strategies for Mitigating Dissolution of Solid Electrolyte Interphases in Sodium‐Ion Batteries Ma, Le Anh; Naylor, Andrew J.; Nyholm, Leif Angewandte Chemie International Edition, Vol. 60, Issue 9 https://doi.org/10.1002/anie.202013803	journal	January 2021
Correlative Electrochemical Microscopy for the Elucidation of the Local Ionic and Electronic Properties of the Solid Electrolyte Interphase in Li‐Ion Batteries Santos, Carla S.; Botz, Alexander; Bandarenka, Aliaksandr S. Angewandte Chemie International Edition, Vol. 61, Issue 26 https://doi.org/10.1002/anie.202202744	journal	May 2022
Dynamics of Solid‐Electrolyte Interphase Formation on Silicon Electrodes Revealed by Combinatorial Electrochemical Screening Martín‐Yerga, Daniel; Milan, David C.; Xu, Xiangdong Angewandte Chemie International Edition, Vol. 61, Issue 34 https://doi.org/10.1002/anie.202207184	journal	July 2022
Surface Degradation of Single‐crystalline Ni‐rich Cathode and Regulation Mechanism by Atomic Layer Deposition in Solid‐State Lithium Batteries Guo, Hui‐Juan; Sun, Yipeng; Zhao, Yang Angewandte Chemie International Edition, Vol. 61, Issue 48 https://doi.org/10.1002/anie.202211626	journal	October 2022
Scanning Electrochemical Cell Microscopy in a Glovebox: Structure‐Activity Correlations in the Early Stages of Solid‐Electrolyte Interphase Formation on Graphite Martín‐Yerga, Daniel; Kang, Minkyung; Unwin, Patrick R. ChemElectroChem, Vol. 8, Issue 22 https://doi.org/10.1002/celc.202101161	journal	October 2021
Analysis of the Stable Interphase Responsible for the Excellent Electrochemical Performance of Graphite Electrodes in Sodium‐Ion Batteries Wang, Zhaohua; Yang, Haoyi; Liu, Yiran Small, Vol. 16, Issue 51 https://doi.org/10.1002/smll.202003268	journal	November 2020
A Comparison of Solid Electrolyte Interphase Formation and Evolution on Highly Oriented Pyrolytic and Disordered Graphite Negative Electrodes in Lithium‐Ion Batteries Zhu, Haoyu; Russell, Joshua A.; Fang, Zongtang Small, Vol. 17, Issue 52 https://doi.org/10.1002/smll.202105292	journal	October 2021
Interfacial Chemistry Effects in the Electrochemical Performance of Silicon Electrodes under Lithium‐Ion Battery Conditions Xu, Xiangdong; Martín‐Yerga, Daniel; Grant, Nicholas E. Small, Vol. 19, Issue 40 https://doi.org/10.1002/smll.202303442	journal	June 2023
Direct Observation of the Growth of Lithium Dendrites on Graphite Anodes by Operando EC-AFM Shen, Cai; Hu, Guohong; Cheong, Ling-Zhi Small Methods, Vol. 2, Issue 2 https://doi.org/10.1002/smtd.201700298	journal	December 2017
Atomic Force Microscopy Voigtländer, Bert NanoScience and Technology https://doi.org/10.1007/978-3-030-13654-3	book	January 2019
In situ electrochemical studies for Li+ ions dissociation from the LiCoO2 electrode by the substrate-generation/tip-collection mode in SECM Xu, Fan; Beak, Byeongjin; Jung, Cheolsoo Journal of Solid State Electrochemistry, Vol. 16, Issue 1 https://doi.org/10.1007/s10008-011-1325-8	journal	February 2011
Volta Potential Evolution of Intermetallics in Aluminum Alloy Microstructure Under Thin Aqueous Adlayers: A combined DFT and Experimental Study Örnek, C.; Liu, M.; Pan, J. Topics in Catalysis, Vol. 61, Issue 9-11 https://doi.org/10.1007/s11244-018-0939-9	journal	April 2018
In-situ nanoscale insights into the evolution of solid electrolyte interphase shells: revealing interfacial degradation in lithium metal batteries Shi, Yang; Liu, Gui-Xian; Wan, Jing Science China Chemistry, Vol. 64, Issue 5 https://doi.org/10.1007/s11426-020-9984-9	journal	March 2021
In situ analysis of dynamic evolution of the additive-regulated cathode processes in quasi-solid-state lithium-metal batteries Tian, Jian-Xin; Guo, Hui-Juan; Wan, Jing Science China Chemistry, Vol. 66, Issue 10 https://doi.org/10.1007/s11426-023-1778-6	journal	September 2023
Automotive Li-Ion Batteries: Current Status and Future Perspectives Ding, Yuanli; Cano, Zachary P.; Yu, Aiping Electrochemical Energy Reviews, Vol. 2, Issue 1 https://doi.org/10.1007/s41918-018-0022-z	journal	January 2019
Advanced Characterizations of Solid Electrolyte Interphases in Lithium-Ion Batteries Chu, Yanli; Shen, Yanbin; Guo, Feng Electrochemical Energy Reviews, Vol. 3, Issue 1 https://doi.org/10.1007/s41918-019-00058-y	journal	November 2019
New insights into the interactions between electrode materials and electrolyte solutions for advanced nonaqueous batteries Aurbach, D.; Markovsky, B.; Levi, M. D. Journal of Power Sources, Vol. 81-82 https://doi.org/10.1016/S0378-7753(99)00187-1	journal	September 1999
In-situ observation of electrolyte-dependent interfacial change of the graphite anode in sodium-ion batteries by atomic force microscopy Zhang, Xin-ren; Yang, Jia-ying; Ren, Zeng-ying New Carbon Materials, Vol. 37, Issue 2 https://doi.org/10.1016/S1872-5805(22)60601-2	journal	April 2022
In-situ EC-AFM and ex-situ XPS characterization to investigate the mechanism of SEI formation in highly concentrated aqueous electrolyte for Li-ion batteries Zhang, Haitao; Wang, Deyu; Shen, Cai Applied Surface Science, Vol. 507 https://doi.org/10.1016/j.apsusc.2019.145059	journal	March 2020
Revealing the cathode electrolyte interphase on Li- and Mn-rich materials by in-situ electrochemical atomic force microscopy Chen, Minjing; Wang, Wenyang; Shi, Zhepu Applied Surface Science, Vol. 600 https://doi.org/10.1016/j.apsusc.2022.154119	journal	October 2022
Localized High-Concentration Sulfone Electrolytes for High-Efficiency Lithium-Metal Batteries Ren, Xiaodi; Chen, Shuru; Lee, Hongkyung Chem, Vol. 4, Issue 8 https://doi.org/10.1016/j.chempr.2018.05.002	journal	August 2018
Evaluating Solid-Electrolyte Interphases for Lithium and Lithium-free Anodes from Nanoindentation Features Wang, Wei-Wei; Gu, Yu; Yan, Hao Chem, Vol. 6, Issue 10 https://doi.org/10.1016/j.chempr.2020.07.014	journal	October 2020
Review on multi-scale models of solid-electrolyte interphase formation Horstmann, Birger; Single, Fabian; Latz, Arnulf Current Opinion in Electrochemistry, Vol. 13 https://doi.org/10.1016/j.coelec.2018.10.013	journal	February 2019
Scanning electrochemical cell microscopy: A natural technique for single entity electrochemistry Wahab, Oluwasegun J.; Kang, Minkyung; Unwin, Patrick R. Current Opinion in Electrochemistry, Vol. 22 https://doi.org/10.1016/j.coelec.2020.04.018	journal	August 2020
Characterization of the solid/electrolyte interphase at hard carbon anodes via scanning (electrochemical) probe microscopy Daboss, S.; Philipp, T.; Palanisamy, K. Electrochimica Acta, Vol. 453 https://doi.org/10.1016/j.electacta.2023.142345	journal	June 2023
Measurement of mechanical and fracture properties of solid electrolyte interphase on lithium metal anodes in lithium ion batteries Yoon, Insun; Jurng, Sunhyung; Abraham, Daniel P. Energy Storage Materials, Vol. 25 https://doi.org/10.1016/j.ensm.2019.10.009	journal	March 2020
Graphite as anode materials: Fundamental mechanism, recent progress and advances Zhang, Hao; Yang, Yang; Ren, Dongsheng Energy Storage Materials, Vol. 36 https://doi.org/10.1016/j.ensm.2020.12.027	journal	April 2021
Unraveling the mechanism of ion and electron migration in composite solid-state electrolyte using conductive atomic force microscopy Shen, Cai; Huang, Yunbo; Yang, Jingru Energy Storage Materials, Vol. 39 https://doi.org/10.1016/j.ensm.2021.04.028	journal	August 2021
Probing depth-dependent inhomogeneous lithium concentration in thick LiNi0.88Co0.09Al0.03O2 cathodes for lithium-ion batteries Choi, Soyoung; Toaran, Weerawat; Kim, Seong Heon Journal of Alloys and Compounds, Vol. 943 https://doi.org/10.1016/j.jallcom.2023.169029	journal	May 2023
Electrolyte-dependent formation of solid electrolyte interphase and ion intercalation revealed by in situ surface characterizations Li, Shiwen; Wang, Chao; Meng, Caixia Journal of Energy Chemistry, Vol. 67 https://doi.org/10.1016/j.jechem.2021.10.003	journal	April 2022
Rapid SECM probing of dissolution of LiCoO2 battery materials in an ionic liquid Snook, Graeme A.; Huynh, Thuy D.; Hollenkamp, Anthony F. Journal of Electroanalytical Chemistry, Vol. 687 https://doi.org/10.1016/j.jelechem.2012.08.021	journal	November 2012
Unraveling the mechanical origin of stable solid electrolyte interphase Gao, Yao; Du, Xiaoqiong; Hou, Zhen Joule, Vol. 5, Issue 7 https://doi.org/10.1016/j.joule.2021.05.015	journal	July 2021
A review of the electrochemical performance of alloy anodes for lithium-ion batteries Zhang, Wei-Jun Journal of Power Sources, Vol. 196, Issue 1 https://doi.org/10.1016/j.jpowsour.2010.07.020	journal	January 2011
Direct observation of important morphology and composition changes at the surface of the CuO conversion material in lithium batteries Martin, Lucile; Martinez, Hervé; Poinot, Delphine Journal of Power Sources, Vol. 248 https://doi.org/10.1016/j.jpowsour.2013.10.015	journal	February 2014
In situ atomic force microscopy nanoindentation of lithiated silicon nanopillars for lithium ion batteries McAllister, Quinn P.; Strawhecker, Kenneth E.; Becker, Collin R. Journal of Power Sources, Vol. 257 https://doi.org/10.1016/j.jpowsour.2014.01.077	journal	July 2014
Component-/structure-dependent elasticity of solid electrolyte interphase layer in Li-ion batteries: Experimental and computational studies Shin, Hosop; Park, Jonghyun; Han, Sangwoo Journal of Power Sources, Vol. 277 https://doi.org/10.1016/j.jpowsour.2014.11.120	journal	March 2015
Measurement on isolated lithium iron phosphate particles reveals heterogeneity in material properties distribution Snowden, Michael E.; Dayeh, Malak; Payne, Nicholas A. Journal of Power Sources, Vol. 325 https://doi.org/10.1016/j.jpowsour.2016.06.081	journal	September 2016
Evolution of solid electrolyte interphase and active material in the silicon wafer model system Stetson, Caleb; Yin, Yanli; Norman, Andrew Journal of Power Sources, Vol. 482 https://doi.org/10.1016/j.jpowsour.2020.228946	journal	January 2021
Local electrical degradations of solid-state electrolyte by nm-scale operando imaging of ionic and electronic transports Jiang, C. -S.; Yin, Y.; Guthrey, H. Journal of Power Sources, Vol. 481 https://doi.org/10.1016/j.jpowsour.2020.229138	journal	January 2021
Interfaces and interphases in batteries Xu, Kang Journal of Power Sources, Vol. 559 https://doi.org/10.1016/j.jpowsour.2023.232652	journal	March 2023
Composite solid electrolytes for all-solid-state lithium batteries Dirican, Mahmut; Yan, Chaoyi; Zhu, Pei Materials Science and Engineering: R: Reports, Vol. 136 https://doi.org/10.1016/j.mser.2018.10.004	journal	April 2019
Revisiting the designing criteria of advanced solid electrolyte interphase on lithium metal anode under practical condition Yuan, Shouyi; Weng, Suting; Wang, Fei Nano Energy, Vol. 83 https://doi.org/10.1016/j.nanoen.2021.105847	journal	May 2021
Promoting the reversibility of lithium ion/lithium metal hybrid graphite anode by regulating solid electrolyte interface Wang, Shuwei; Liu, Dongqing; Cai, Xingke Nano Energy, Vol. 90 https://doi.org/10.1016/j.nanoen.2021.106510	journal	December 2021
Development of solid-state electrolytes for sodium-ion battery–A short review Wang, Yumei; Song, Shufeng; Xu, Chaohe Nano Materials Science, Vol. 1, Issue 2 https://doi.org/10.1016/j.nanoms.2019.02.007	journal	June 2019
Force measurements with the atomic force microscope: Technique, interpretation and applications Butt, Hans-Jürgen; Cappella, Brunero; Kappl, Michael Surface Science Reports, Vol. 59, Issue 1-6 https://doi.org/10.1016/j.surfrep.2005.08.003	journal	October 2005
Scanning electrochemical microscopy. Introduction and principles Bard, Allen J.; Fan, Fu Ren F.; Kwak, Juhyoun. Analytical Chemistry, Vol. 61, Issue 2 https://doi.org/10.1021/ac00177a011	journal	January 1989
Localized High Resolution Electrochemistry and Multifunctional Imaging: Scanning Electrochemical Cell Microscopy Ebejer, Neil; Schnippering, Mathias; Colburn, Alexander W. Analytical Chemistry, Vol. 82, Issue 22 https://doi.org/10.1021/ac102191u	journal	November 2010
Origins of Nanoscale Damage to Glass-Sealed Platinum Electrodes with Submicrometer and Nanometer Size Nioradze, Nikoloz; Chen, Ran; Kim, Jiyeon Analytical Chemistry, Vol. 85, Issue 13 https://doi.org/10.1021/ac401316n	journal	June 2013
Scanning Micropipet Contact Method for High-Resolution Imaging of Electrode Surface Redox Activity Williams, Cara G.; Edwards, Martin A.; Colley, Anna L. Analytical Chemistry, Vol. 81, Issue 7 https://doi.org/10.1021/ac802114r	journal	March 2009
Scanning Electrochemical Microscopy: A Comprehensive Review of Experimental Parameters from 1989 to 2015 Polcari, David; Dauphin-Ducharme, Philippe; Mauzeroll, Janine Chemical Reviews, Vol. 116, Issue 22 https://doi.org/10.1021/acs.chemrev.6b00067	journal	October 2016
Experimental Visualization of Commercial Lithium Ion Battery Cathodes: Distinguishing Between the Microstructure Components Using Atomic Force Microscopy Terreblanche, J. S.; Thompson, D. L.; Aldous, I. M. The Journal of Physical Chemistry C, Vol. 124, Issue 27 https://doi.org/10.1021/acs.jpcc.0c02713	journal	June 2020
Visualizing Local Electrical Properties of Composite Electrodes in Sulfide All-Solid-State Batteries by Scanning Probe Microscopy Otoyama, Misae; Yamaoka, Takehiro; Ito, Hiroyuki The Journal of Physical Chemistry C, Vol. 125, Issue 5 https://doi.org/10.1021/acs.jpcc.0c10148	journal	January 2021
Direct Correlation between Local Surface Potential Measured by Kelvin Probe Force Microscope and Electrochemical Potential of LiNi _0.80 Co _0.15 Al _0.05 O ₂ Cathode at Different State of Charge Zhu, Xinhua; Revilla, Reynier I.; Hubin, Annick The Journal of Physical Chemistry C, Vol. 122, Issue 50 https://doi.org/10.1021/acs.jpcc.8b10364	journal	December 2018
Innermost Ion Association Configuration Is a Key Structural Descriptor of Ionic Liquids at Electrified Interfaces Panse, Kaustubh S.; Wu, Haiyi; Zhou, Shan The Journal of Physical Chemistry Letters, Vol. 13, Issue 40 https://doi.org/10.1021/acs.jpclett.2c02768	journal	October 2022
Real-Time Observation of Li Deposition on a Li Electrode with Operand Atomic Force Microscopy and Surface Mechanical Imaging Kitta, Mitsunori; Sano, Hikaru Langmuir, Vol. 33, Issue 8 https://doi.org/10.1021/acs.langmuir.6b04651	journal	February 2017
Molecular-Resolution Imaging of Interfacial Solvation of Electrolytes for Lithium-Ion Batteries by Frequency Modulation Atomic Force Microscopy Yamagishi, Yuji; Kominami, Hiroaki; Kobayashi, Kei Nano Letters, Vol. 22, Issue 24 https://doi.org/10.1021/acs.nanolett.2c03325	journal	December 2022
Effect of Fluoroethylene Carbonate on Solid Electrolyte Interphase Formation of the SiO/C Anode Observed by In Situ Atomic Force Microscopy Zhao, Rui; Wang, Shuwei; Liu, Dongqing ACS Applied Energy Materials, Vol. 4, Issue 1 https://doi.org/10.1021/acsaem.0c02399	journal	January 2021
Operando Electrochemical Atomic Force Microscopy of Solid–Electrolyte Interphase Formation on Graphite Anodes: The Evolution of SEI Morphology and Mechanical Properties Zhang, Zhenyu; Smith, Keenan; Jervis, Rhodri ACS Applied Materials & Interfaces, Vol. 12, Issue 31 https://doi.org/10.1021/acsami.0c11190	journal	July 2020
Understanding Degradation at the Lithium-Ion Battery Cathode/Electrolyte Interface: Connecting Transition-Metal Dissolution Mechanisms to Electrolyte Composition Huang, Di; Engtrakul, Chaiwat; Nanayakkara, Sanjini ACS Applied Materials & Interfaces, Vol. 13, Issue 10 https://doi.org/10.1021/acsami.0c22235	journal	March 2021
Impact of Charge Voltage on Factors Influencing Capacity Fade in Layered NMC622: Multimodal X-ray and Electrochemical Characterization Quilty, Calvin D.; Wheeler, Garrett P.; Wang, Lei ACS Applied Materials & Interfaces, Vol. 13, Issue 43 https://doi.org/10.1021/acsami.1c14272	journal	October 2021
Insights into the Lithium Nucleation and Plating/Stripping Behavior in Ionic Liquid-Based Electrolytes Stępień, Dominik; Wolff, Beatrice; Diemant, Thomas ACS Applied Materials & Interfaces, Vol. 15, Issue 21 https://doi.org/10.1021/acsami.3c01722	journal	May 2023
Localized Mechanical Stress Induced Ionic Redistribution in a Layered LiCoO₂ Cathode Yao, Wentao; Long, Fei; Shahbazian-Yassar, Reza ACS Applied Materials & Interfaces, Vol. 8, Issue 43 https://doi.org/10.1021/acsami.6b07491	journal	October 2016
In Situ Visualized Cathode Electrolyte Interphase on LiCoO ₂ in High Voltage Cycling Lu, Wei; Zhang, Jiansheng; Xu, Jingjing ACS Applied Materials & Interfaces, Vol. 9, Issue 22 https://doi.org/10.1021/acsami.7b03024	journal	May 2017
In Situ Atomic Force Microscopic Studies of Single Tin Nanoparticle: Sodiation and Desodiation in Liquid Electrolyte Han, Mo; Zhu, Chenbo; Zhao, Qing ACS Applied Materials & Interfaces, Vol. 9, Issue 34 https://doi.org/10.1021/acsami.7b08870	journal	August 2017
In Situ Observation of Sodium Dendrite Growth and Concurrent Mechanical Property Measurements Using an Environmental Transmission Electron Microscopy–Atomic Force Microscopy (ETEM-AFM) Platform Liu, Qiunan; Zhang, Liqiang; Sun, Haiming ACS Energy Letters, Vol. 5, Issue 8 https://doi.org/10.1021/acsenergylett.0c01214	journal	July 2020
How Comparable Are Sodium-Ion Batteries to Lithium-Ion Counterparts? Abraham, K. M. ACS Energy Letters, Vol. 5, Issue 11 https://doi.org/10.1021/acsenergylett.0c02181	journal	October 2020
Spatially Resolved Potential and Li-Ion Distributions Reveal Performance-Limiting Regions in Solid-State Batteries Fuller, Elliot J.; Strelcov, Evgheni; Weaver, Jamie L. ACS Energy Letters, Vol. 6, Issue 11 https://doi.org/10.1021/acsenergylett.1c01960	journal	October 2021
Emerging Era of Electrolyte Solvation Structure and Interfacial Model in Batteries Cheng, Haoran; Sun, Qujiang; Li, Leilei ACS Energy Letters, Vol. 7, Issue 1 https://doi.org/10.1021/acsenergylett.1c02425	journal	January 2022
Solubility of the Solid Electrolyte Interphase (SEI) in Sodium Ion Batteries Mogensen, Ronnie; Brandell, Daniel; Younesi, Reza ACS Energy Letters, Vol. 1, Issue 6 https://doi.org/10.1021/acsenergylett.6b00491	journal	November 2016
New Insights on Graphite Anode Stability in Rechargeable Batteries: Li Ion Coordination Structures Prevail over Solid Electrolyte Interphases Ming, Jun; Cao, Zhen; Wahyudi, Wandi ACS Energy Letters, Vol. 3, Issue 2 https://doi.org/10.1021/acsenergylett.7b01177	journal	January 2018
Three-Dimensional Molecular Mapping of Ionic Liquids at Electrified Interfaces Zhou, Shan; Panse, Kaustubh S.; Motevaselian, Mohammad Hossein ACS Nano, Vol. 14, Issue 12 https://doi.org/10.1021/acsnano.0c07957	journal	November 2020
Black Phosphorus Degradation during Intercalation and Alloying in Batteries Said, Samia; Zhang, Zhenyu; Shutt, Rebecca R. C. ACS Nano, Vol. 17, Issue 7 https://doi.org/10.1021/acsnano.2c08776	journal	March 2023
Real-Space Charge Density Profiling of Electrode–Electrolyte Interfaces with Angstrom Depth Resolution Bonagiri, Lalith Krishna Samanth; Panse, Kaustubh S.; Zhou, Shan ACS Nano, Vol. 16, Issue 11 https://doi.org/10.1021/acsnano.2c10819	journal	November 2022
Elucidating the Phase Transformation of Li ₄ Ti ₅ O ₁₂ Lithiation at the Nanoscale Verde, Michael G.; Baggetto, Loïc; Balke, Nina ACS Nano, Vol. 10, Issue 4 https://doi.org/10.1021/acsnano.5b07875	journal	March 2016
On the Theoretical Capacity/Energy of Lithium Batteries and Their Counterparts Eftekhari, Ali ACS Sustainable Chemistry & Engineering, Vol. 7, Issue 4 https://doi.org/10.1021/acssuschemeng.7b04330	journal	March 2018
Challenges for Rechargeable Li Batteries Goodenough, John B.; Kim, Youngsik Chemistry of Materials, Vol. 22, Issue 3, p. 587-603 https://doi.org/10.1021/cm901452z	journal	February 2010
Nonaqueous Liquid Electrolytes for Lithium-Based Rechargeable Batteries Xu, Kang Chemical Reviews, Vol. 104, Issue 10, p. 4303-4418 https://doi.org/10.1021/cr030203g	journal	October 2004
Electrolytes and Interphases in Li-Ion Batteries and Beyond Xu, Kang Chemical Reviews, Vol. 114, Issue 23 https://doi.org/10.1021/cr500003w	journal	October 2014
Research Development on Sodium-Ion Batteries Yabuuchi, Naoaki; Kubota, Kei; Dahbi, Mouad Chemical Reviews, Vol. 114, Issue 23 https://doi.org/10.1021/cr500192f	journal	October 2014
Reversible Switch in Charge Storage Enabled by Selective Ion Transport in Solid Electrolyte Interphase Tao, Lei; Russell, Joshua A.; Xia, Dawei Journal of the American Chemical Society, Vol. 145, Issue 30 https://doi.org/10.1021/jacs.3c03429	journal	July 2023
Direct Observation of Inhomogeneous Solid Electrolyte Interphase on MnO Anode with Atomic Force Microscopy and Spectroscopy Zhang, Jie; Wang, Rui; Yang, Xiaocheng Nano Letters, Vol. 12, Issue 4 https://doi.org/10.1021/nl300570d	journal	January 2012
In Situ and Quantitative Characterization of Solid Electrolyte Interphases Cresce, Arthur v.; Russell, Selena M.; Baker, David R. Nano Letters, Vol. 14, Issue 3 https://doi.org/10.1021/nl404471v	journal	February 2014
Atomic Force Microscopy Studies on Molybdenum Disulfide Flakes as Sodium-Ion Anodes Lacey, Steven D.; Wan, Jiayu; Cresce, Arthur von Wald Nano Letters, Vol. 15, Issue 2 https://doi.org/10.1021/nl503871s	journal	January 2015
Nanoscale Mapping of Lithium-Ion Diffusion in a Cathode within an All-Solid-State Lithium-Ion Battery by Advanced Scanning Probe Microscopy Techniques Zhu, Jing; Lu, Li; Zeng, Kaiyang ACS Nano, Vol. 7, Issue 2 https://doi.org/10.1021/nn305648j	journal	January 2013
Issues and challenges facing rechargeable lithium batteries Tarascon, J.-M.; Armand, M. Nature, Vol. 414, Issue 6861, p. 359-367 https://doi.org/10.1038/35104644	journal	November 2001
Building better batteries Armand, M.; Tarascon, J.-M. Nature, Vol. 451, Issue 7179, p. 652-657 https://doi.org/10.1038/451652a	journal	February 2008
Extending the low-temperature operation of sodium metal batteries combining linear and cyclic ether-based electrolyte solutions Wang, Chuanlong; Thenuwara, Akila C.; Luo, Jianmin Nature Communications, Vol. 13, Issue 1 https://doi.org/10.1038/s41467-022-32606-4	journal	August 2022
Nanoarchitecture factors of solid electrolyte interphase formation via 3D nano-rheology microscopy and surface force-distance spectroscopy Chen, Yue; Wu, Wenkai; Gonzalez-Munoz, Sergio Nature Communications, Vol. 14, Issue 1 https://doi.org/10.1038/s41467-023-37033-7	journal	March 2023
Tailoring electrolyte solvation for Li metal batteries cycled at ultra-low temperature Holoubek, John; Liu, Haodong; Wu, Zhaohui Nature Energy, Vol. 6, Issue 3 https://doi.org/10.1038/s41560-021-00783-z	journal	February 2021
Engineering high-energy-density sodium battery anodes for improved cycling with superconcentrated ionic-liquid electrolytes Rakov, Dmitrii A.; Chen, Fangfang; Ferdousi, Shammi A. Nature Materials, Vol. 19, Issue 10 https://doi.org/10.1038/s41563-020-0673-0	journal	May 2020
Multi-characterization of LiCoO2 cathode films using advanced AFM-based techniques with high resolution Wu, Jiaxiong; Yang, Shan; Cai, Wei Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-11623-0	journal	September 2017
Solid-electrolyte interphase nucleation and growth on carbonaceous negative electrodes for Li-ion batteries visualized with in situ atomic force microscopy Luchkin, Sergey Yu.; Lipovskikh, Svetlana A.; Katorova, Natalia S. Scientific Reports, Vol. 10, Issue 1 https://doi.org/10.1038/s41598-020-65552-6	journal	May 2020
Dynamically visualizing battery reactions by operando Kelvin probe force microscopy Masuda, Hideki; Matsushita, Kyosuke; Ito, Daigo Communications Chemistry, Vol. 2, Issue 1 https://doi.org/10.1038/s42004-019-0245-x	journal	December 2019
Direct observation of lithium-ion transport under an electrical field in LixCoO2 nanograins Zhu, Xiaojian; Ong, Chin Shen; Xu, Xiaoxiong Scientific Reports, Vol. 3, Issue 1 https://doi.org/10.1038/srep01084	journal	January 2013
Electrolytes, Interfaces and Interphases Xu, Kang https://doi.org/10.1039/9781837671311	book	April 2023
3D visualization of inhomogeneous multi-layered structure and Young's modulus of the solid electrolyte interphase (SEI) on silicon anodes for lithium ion batteries Zheng, Jieyun; Zheng, Hao; Wang, Rui Phys. Chem. Chem. Phys., Vol. 16, Issue 26 https://doi.org/10.1039/C4CP01968G	journal	January 2014
Direct visualization of solid electrolyte interphase on Li ₄ Ti ₅ O ₁₂ by in situ AFM Wang, Shuwei; Yang, Kai; Gao, Fei RSC Advances, Vol. 6, Issue 81 https://doi.org/10.1039/C6RA16208H	journal	January 2016
Dendrite formation in silicon anodes of lithium-ion batteries Selis, Luis A.; Seminario, Jorge M. RSC Advances, Vol. 8, Issue 10 https://doi.org/10.1039/C7RA12690E	journal	January 2018
Probing the reversibility and kinetics of Li ⁺ during SEI formation and (de)intercalation on edge plane graphite using ion-sensitive scanning electrochemical microscopy Gossage, Zachary T.; Hui, Jingshu; Zeng, Yunxiong Chemical Science, Vol. 10, Issue 46 https://doi.org/10.1039/C9SC03569A	journal	January 2019
Optimized atomic layer deposition of homogeneous, conductive Al₂O₃ coatings for high-nickel NCM containing ready-to-use electrodes Negi, Rajendra S.; Culver, Sean P.; Wiche, Miguel Physical Chemistry Chemical Physics, Vol. 23, Issue 11 https://doi.org/10.1039/D0CP06422J	journal	January 2021
Nanoscale observation of the solid electrolyte interface and lithium dendrite nucleation–growth process during the initial lithium electrodeposition Wang, Shuwei; Yin, Xiaoguang; Liu, Dongqing Journal of Materials Chemistry A, Vol. 8, Issue 35 https://doi.org/10.1039/D0TA06141G	journal	January 2020
Practical guidelines for the use of scanning electrochemical cell microscopy (SECCM) Jayamaha, Gunani; Maleki, Mahin; Bentley, Cameron L. The Analyst, Vol. 149, Issue 9 https://doi.org/10.1039/D4AN00117F	journal	January 2024
Kelvin probe force microscopy Nonnenmacher, M.; O’Boyle, M. P.; Wickramasinghe, H. K. Applied Physics Letters, Vol. 58, Issue 25 https://doi.org/10.1063/1.105227	journal	June 1991
Prospects for the Application of Scanning Electrochemical Microscopy in Ionic Liquids Carano, Maurizio; Bond, Alan M. Australian Journal of Chemistry, Vol. 60, Issue 1 https://doi.org/10.1071/CH06269	journal	January 2007
Mechanical studies of the solid electrolyte interphase on anodes in lithium and lithium ion batteries McBrayer, Josefine D.; Apblett, Christopher A.; Harrison, Katharine L. Nanotechnology, Vol. 32, Issue 50 https://doi.org/10.1088/1361-6528/ac17fe	journal	September 2021
Atomic-Scale Distribution of Water Molecules at the Mica-Water Interface Visualized by Three-Dimensional Scanning Force Microscopy Fukuma, Takeshi; Ueda, Yasumasa; Yoshioka, Shunsuke Physical Review Letters, Vol. 104, Issue 1 https://doi.org/10.1103/PhysRevLett.104.016101	journal	January 2010
Surface Studies by Scanning Tunneling Microscopy Binnig, G.; Rohrer, H.; Gerber, Ch. Physical Review Letters, Vol. 49, Issue 1 https://doi.org/10.1103/PhysRevLett.49.57	journal	July 1982
Atomic Force Microscope Binnig, G.; Quate, C. F.; Gerber, Ch. Physical Review Letters, Vol. 56, Issue 9 https://doi.org/10.1103/PhysRevLett.56.930	journal	March 1986
High resolution atomic force microscopy potentiometry Weaver, J. M. R. Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 9, Issue 3 https://doi.org/10.1116/1.585423	journal	May 1991
Reversible planar gliding and microcracking in a single-crystalline Ni-rich cathode Bi, Yujing; Tao, Jinhui; Wu, Yuqin Science, Vol. 370, Issue 6522 https://doi.org/10.1126/science.abc3167	journal	December 2020
Designing better electrolytes Meng, Y. Shirley; Srinivasan, Venkat; Xu, Kang Science, Vol. 378, Issue 6624 https://doi.org/10.1126/science.abq3750	journal	December 2022
Scanning Electrochemical Cell Microscopy: A Versatile Technique for Nanoscale Electrochemistry and Functional Imaging Ebejer, Neil; Güell, Aleix G.; Lai, Stanley C. S. Annual Review of Analytical Chemistry, Vol. 6, Issue 1 https://doi.org/10.1146/annurev-anchem-062012-092650	journal	June 2013
Electrochemical Imaging of Interfaces in Energy Storage via Scanning Probe Methods: Techniques, Applications, and Prospects Mishra, Abhiroop; Sarbapalli, Dipobrato; Rodríguez, Oliver Annual Review of Analytical Chemistry, Vol. 16, Issue 1 https://doi.org/10.1146/annurev-anchem-091422-110703	journal	June 2023
In Situ Electrochemical Atomic Force Microscope Study on Graphite Electrodes Hirasawa, Karen A.; Sato, Tomohiro; Asahina, Hitoshi Journal of The Electrochemical Society, Vol. 144, Issue 4 https://doi.org/10.1149/1.1837560	journal	April 1997
Advanced Model for Solid Electrolyte Interphase Electrodes in Liquid and Polymer Electrolytes Peled, E. Journal of The Electrochemical Society, Vol. 144, Issue 8 https://doi.org/10.1149/1.1837858	journal	January 1997
Electrochemistry of Highly Ordered Pyrolytic Graphite Surface Film Formation Observed by Atomic Force Microscopy Chu, Andrew C.; Josefowicz, Jack Y.; Farrington, Gregory C. Journal of The Electrochemical Society, Vol. 144, Issue 12 https://doi.org/10.1149/1.1838160	journal	December 1997
The Impact of Elastic Deformation on Deposition Kinetics at Lithium/Polymer Interfaces Monroe, Charles; Newman, John Journal of The Electrochemical Society, Vol. 152, Issue 2 https://doi.org/10.1149/1.1850854	journal	January 2005
Applications and Limitations of Scanning Kelvin Probe Force Microscopy for the Surface Analysis of Aluminum Alloys Muster, T. H.; Hughes, A. E. Journal of The Electrochemical Society, Vol. 153, Issue 11 https://doi.org/10.1149/1.2349356	journal	January 2006
Highly Sensitive Detection and Mapping of Incipient and Steady-State Oxygen Evolution from Operating Li-Ion Battery Cathodes via Scanning Electrochemical Microscopy Mishra, Abhiroop; Sarbapalli, Dipobrato; Hossain, Md. Sazzad Journal of The Electrochemical Society, Vol. 169, Issue 8 https://doi.org/10.1149/1945-7111/ac857e	journal	August 2022
In Situ Investigation of Lattice Oxygen Loss from Preferentially Faceted Electrodeposited LiCoO₂ via Scanning Electrochemical Microscopy Mishra, Abhiroop; Lin, Jr-Wen; Zahiri, Beniamin Journal of The Electrochemical Society, Vol. 171, Issue 5 https://doi.org/10.1149/1945-7111/ad4f22	journal	May 2024
Toward Improving Ambient Volta Potential Measurements with SKPFM for Corrosion Studies Efaw, Corey M.; da Silva, Thiago; Davis, Paul H. Journal of The Electrochemical Society, Vol. 166, Issue 11 https://doi.org/10.1149/2.0041911jes	journal	January 2019
Recent development of PeakForce Tapping mode atomic force microscopy and its applications on nanoscience Xu, Ke; Sun, Weihang; Shao, Yongjian Nanotechnology Reviews, Vol. 7, Issue 6 https://doi.org/10.1515/ntrev-2018-0086	journal	October 2018
The Solid Electrolyte Interphase – The Most Important and the Least Understood Solid Electrolyte in Rechargeable Li Batteries Winter, Martin Zeitschrift für Physikalische Chemie, Vol. 223, Issue 10-11 https://doi.org/10.1524/zpch.2009.6086	journal	December 2009
A Review: Scanning Electrochemical Microscopy (SECM) for Visualizing the Real-Time Local Catalytic Activity Preet, Anant; Lin, Tzu-En Catalysts, Vol. 11, Issue 5 https://doi.org/10.3390/catal11050594	journal	May 2021
Visualization of solvation structure on Li₄Ti₅O₁₂(111)/ ionic liquid-based electrolyte interface by atomic force microscopy Bao, Yifan; Kitta, Mitsunori; Ichii, Takashi Japanese Journal of Applied Physics, Vol. 60, Issue SE https://doi.org/10.35848/1347-4065/abf3a3	journal	April 2021
Volta Potentials Measured by Scanning Kelvin Probe Force Microscopy as Relevant to Corrosion of Magnesium Alloys Hurley, M. F.; Efaw, C. M.; Davis, P. H. CORROSION, Vol. 71, Issue 2 https://doi.org/10.5006/1432	journal	February 2015
Understanding the Feedback Circuit in an Atomic Force Microscope An, Sangmin Applied Science and Convergence Technology, Vol. 31, Issue 4 https://doi.org/10.5757/ASCT.2022.31.4.99	journal	July 2022

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