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On the pressure induced phase of Na{sub 2}CsC{sub 60}

Conference ·
OSTI ID:247416
;  [1];  [2];  [3];  [4];  [5]
  1. Sandia National Labs., Albuquerque, NM (United States)
  2. Argonne National Lab., IL (United States)
  3. Lawrence Livermore National Lab., CA (United States)
  4. Maryland Univ., College Park, MD (United States)
  5. Pennsylvania Univ., Philadelphia, PA (United States)

Neutron powder diffraction at pressures to 6 kbar in gaseous Ne has been used to study the pressure-induced phase transition and compressibilities of Na{sub 2}CsC{sub 60}. The pressure-induced phase can be achieved by compression to about 5 kbar at room temperature. If cooled, this phase can be retained below 200 K upon release of the pressure. The structure is orthorhombic as previously reported (but may differ in its detailed crystal structure) with lattice constants near 80 K and ambient pressure of a=9.385 A, b=10.06 A, and c=14.36 A. Corresponding linear compressibilities are 0.0004, 0014, and 0.0017 kbar{sup -1}, respectively. Identical pressure temperature cycling results in a superconductor with an unexpectedly low pressure dependence for {Tc} while in this phase. Models for the superconducting behavior of this compound are discussed.

Research Organization:
Sandia National Labs., Albuquerque, NM (United States); Argonne National Lab., IL (United States); Lawrence Livermore National Lab., CA (United States); Pennsylvania Univ., Philadelphia, PA (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC04-94AL85000; FG02-86ER45254; W-7405-ENG-48; W-31109-ENG-38
OSTI ID:
247416
Report Number(s):
SAND--96-1176C; ANL/MSD/CP--90766; CONF-960502--14; ON: DE96010563
Country of Publication:
United States
Language:
English